(μ-1,2-bis(diphenylphosphino)ethane)[Mo(CO)4(tert-butyl isocyanide)]2

Base Information

Chemical Name:(μ-1,2-bis(diphenylphosphino)ethane)[Mo(CO)4(tert-butyl isocyanide)]2
CAS No.:89232-07-5
Molecular Formula:C₄₄H₄₂Mo₂N₂O₈P₂
Molecular Weight:980.654
Hs Code.:

Synonyms:(μ-1,2-bis(diphenylphosphino)ethane)[Mo(CO)4(tert-butyl isocyanide)]2

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Chemical Property of (μ-1,2-bis(diphenylphosphino)ethane)[Mo(CO)4(tert-butyl isocyanide)]2

Chemical Property:

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Technology Process of (μ-1,2-bis(diphenylphosphino)ethane)[Mo(CO)4(tert-butyl isocyanide)]2

There total 2 articles about (μ-1,2-bis(diphenylphosphino)ethane)[Mo(CO)4(tert-butyl isocyanide)]2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 89255-65-2
(Ph4P)[μ-HMo2(CO)10]

: 89232-07-5
(μ-1,2-bis(diphenylphosphino)ethane)[Mo(CO)4(tert-butyl isocyanide)]2

Guidance literature:: Multi-step reaction with 2 steps

1: bis-(diphenylphosphino)-ethane / tetrahydrofuran

2: CF₃COOH / dichloromethane

With bis-(diphenylphosphino)-ethane; CF₃COOH; In tetrahydrofuran; dichloromethane;
DOI:10.1021/ja00321a016

Reference yield:

: 89232-03-1
(Ph4P)[(μ-H)(μ-1,2-bis(diphenylphosphino)ethane)Mo2(CO)8]

: 119072-55-8,7188-38-7
tert-butylisonitrile

: 89232-07-5
(μ-1,2-bis(diphenylphosphino)ethane)[Mo(CO)4(tert-butyl isocyanide)]2

Guidance literature:: With CF₃COOH; In dichloromethane; under N2, with rapid stirring CF3COOH syringed in soln. of reagents in CH2Cl2, react. was complete within 15 min; product pptd. by addn. of MeCN; elem. anal.;
DOI:10.1021/ja00321a016