benzo[cyano-¹⁴C]nitrile

Base Information

• Chemical Name: benzo[cyano-¹⁴C]nitrile
• CAS No.: 24420-97-1
• Molecular Formula: C₇H₅N
• Molecular Weight: 105.112
• Mol file: 24420-97-1.mol

Synonyms:benzo[cyano-¹⁴C]nitrile

Chemical Property of benzo[cyano-¹⁴C]nitrile

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of benzo[cyano-¹⁴C]nitrile

There total 4 articles about benzo[cyano-¹⁴C]nitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.3%

zinc [14C2]cyanide + iodobenzene (591-50-4) → benzo[cyano-14C]nitrile (24420-97-1)

Guidance literature:

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; In N,N-dimethyl-formamide; at 80 ℃; Inert atmosphere;

DOI:10.1002/jlcr.3110

Reference yield:

iodobenzene (591-50-4) + [14C]potassium cyanide (5373-08-0) → benzo[cyano-14C]nitrile (24420-97-1)

Guidance literature:

With copper(l) iodide; In N,N-dimethyl-formamide; for 10h; Heating;

DOI:10.1002/jlcr.1032

Reference yield:

iodobenzene (591-50-4) + [14C]copper cyanide (17410-52-5) → benzo[cyano-14C]nitrile (24420-97-1)

Guidance literature:

In N,N-dimethyl-formamide; for 7h; Heating;

DOI:10.1002/jlcr.794

upstream raw materials:

iodobenzene

[¹⁴C]copper cyanide

[14C]potassium cyanide

Downstream raw materials:

[carbonyl‐¹⁴C] benzaldehyde

[carbonyl-14C]benzamide