11-bromoundecanoic acid (4-{3-[4-(2-benzhydryloxyethyl)piperazin-1-yl]propyl}phenyl)amide

Base Information

Chemical Name:11-bromoundecanoic acid (4-{3-[4-(2-benzhydryloxyethyl)piperazin-1-yl]propyl}phenyl)amide
CAS No.:374808-68-1
Molecular Formula:C₃₉H₅₄BrN₃O₂
Molecular Weight:676.781
Hs Code.:

Synonyms:11-bromoundecanoic acid (4-{3-[4-(2-benzhydryloxyethyl)piperazin-1-yl]propyl}phenyl)amide

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Chemical Property of 11-bromoundecanoic acid (4-{3-[4-(2-benzhydryloxyethyl)piperazin-1-yl]propyl}phenyl)amide

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Technology Process of 11-bromoundecanoic acid (4-{3-[4-(2-benzhydryloxyethyl)piperazin-1-yl]propyl}phenyl)amide

There total 4 articles about 11-bromoundecanoic acid (4-{3-[4-(2-benzhydryloxyethyl)piperazin-1-yl]propyl}phenyl)amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 28.0%

: 2834-05-1
11-bromoundecanoic acid

: 127139-25-7
1-[2-[bis(phenyl)methoxy]ethyl]-4-(3-(4-aminophenyl)propyl)piperazine

: 374808-68-1
11-bromoundecanoic acid (4-{3-[4-(2-benzhydryloxyethyl)piperazin-1-yl]propyl}phenyl)amide

Guidance literature:: 11-bromoundecanoic acid; With 1,1'-carbonyldiimidazole; In tetrahydrofuran; at 20 ℃; for 1h;

1-[2-[bis(phenyl)methoxy]ethyl]-4-(3-(4-aminophenyl)propyl)piperazine; In tetrahydrofuran; at 20 ℃; for 96h;
DOI:10.1016/S0040-4020(03)01179-7

Reference yield:

: 15949-84-5
11-bromoundecanoyl chloride

: 127139-25-7
1-[2-[bis(phenyl)methoxy]ethyl]-4-(3-(4-aminophenyl)propyl)piperazine

: 374808-68-1
11-bromoundecanoic acid (4-{3-[4-(2-benzhydryloxyethyl)piperazin-1-yl]propyl}phenyl)amide

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃; for 96h;
DOI:10.1016/S0040-4020(03)01179-7

Reference yield:

: 374808-04-5
1-[2-[bisphenylmethoxy]ethyl]-4-(3-(4-nitrophenyl)-1-oxopropyl)piperazine

: 374808-68-1
11-bromoundecanoic acid (4-{3-[4-(2-benzhydryloxyethyl)piperazin-1-yl]propyl}phenyl)amide

Guidance literature:: Multi-step reaction with 2 steps

1.1: 78.6 percent / SnCl₂*2H₂O / ethanol / 1.5 h / Heating

2.1: 1,1'-carbonyldiimidazole / tetrahydrofuran / 1 h / 20 °C

2.2: 28 percent / tetrahydrofuran / 96 h / 20 °C

With 1,1'-carbonyldiimidazole; tin(ll) chloride; In tetrahydrofuran; ethanol;
DOI:10.1016/S0040-4020(03)01179-7