(E)-6-Benzenesulfonyl-2-(1-ethoxy-ethoxy)-2-isobutyl-4-methyl-hex-4-enenitrile

Base Information

Chemical Name:(E)-6-Benzenesulfonyl-2-(1-ethoxy-ethoxy)-2-isobutyl-4-methyl-hex-4-enenitrile
CAS No.:79998-92-8
Molecular Formula:C₂₁H₃₁NO₄S
Molecular Weight:393.547
Hs Code.:

Synonyms:(E)-6-Benzenesulfonyl-2-(1-ethoxy-ethoxy)-2-isobutyl-4-methyl-hex-4-enenitrile

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (E)-6-Benzenesulfonyl-2-(1-ethoxy-ethoxy)-2-isobutyl-4-methyl-hex-4-enenitrile

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Technology Process of (E)-6-Benzenesulfonyl-2-(1-ethoxy-ethoxy)-2-isobutyl-4-methyl-hex-4-enenitrile

There total 2 articles about (E)-6-Benzenesulfonyl-2-(1-ethoxy-ethoxy)-2-isobutyl-4-methyl-hex-4-enenitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 16627-79-5
(E) 3-methyl-1,3-butadienyl phenyl sulfide

: 79998-92-8
(E)-6-Benzenesulfonyl-2-(1-ethoxy-ethoxy)-2-isobutyl-4-methyl-hex-4-enenitrile

Guidance literature:: Multi-step reaction with 2 steps

1: m-chloroperbenzoic acid / various solvent(s) / 2 h / 0 °C

2: 1.) LDA / 1.) THF, -78 deg C,5 min, 2.) -78 deg C, 1 h; -78 deg C -> 0 deg C, 1 h; 0 deg C , 1 h

With 3-chloro-benzenecarboperoxoic acid; lithium diisopropyl amide; In various solvent(s);

Reference yield:

: 63184-63-4
2-(1-Ethoxy-ethoxy)-4-methyl-pentanenitrile

: 80283-59-6
(E)-((3-methylbuta-1,3-dien-1-yl)sulfonyl)benzene

: 79998-92-8
(E)-6-Benzenesulfonyl-2-(1-ethoxy-ethoxy)-2-isobutyl-4-methyl-hex-4-enenitrile

Guidance literature:: With lithium diisopropyl amide; Yield given. Multistep reaction; 1.) THF, -78 deg C,5 min, 2.) -78 deg C, 1 h; -78 deg C -> 0 deg C, 1 h; 0 deg C , 1 h;

Reference yield:

: 79998-92-8
(E)-6-Benzenesulfonyl-2-(1-ethoxy-ethoxy)-2-isobutyl-4-methyl-hex-4-enenitrile

: 23985-25-3
2,6-dimethyl-octa-5,7-dien-4-one

Guidance literature:: Multi-step reaction with 3 steps

1: 5percent aq. sulfuric acid / methanol / 0.17 h

2: 180 mg / 0.5N aq. sodium hydroxide / diethyl ether / 0.17 h

3: N-aq. sodium hydroxide / diethyl ether / 1 h

With sodium hydroxide; sulfuric acid; In methanol; diethyl ether;