C₁₅H₂₇Cl₂NSi₂

Base Information

• Chemical Name: C₁₅H₂₇Cl₂NSi₂
• CAS No.: 1309944-27-1
• Molecular Formula: C₁₅H₂₇Cl₂NSi₂
• Molecular Weight: 348.463
• Mol file: 1309944-27-1.mol

Synonyms:C₁₅H₂₇Cl₂NSi₂

Chemical Property of C₁₅H₂₇Cl₂NSi₂

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₅H₂₇Cl₂NSi₂

There total 2 articles about C₁₅H₂₇Cl₂NSi₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.1%

N-trimethylsilyl-2,6-diisopropylaniline (78923-65-6) → C15H27Cl2NSi2 (1309944-27-1)

Guidance literature:

N-trimethylsilyl-2,6-diisopropylaniline; With n-butyllithium; In diethyl ether; hexane; at -78 - 20 ℃; Inert atmosphere;

With trichlorosilane; In diethyl ether; hexane; at -78 - 20 ℃; Inert atmosphere;

DOI:10.1002/asia.201100022

Reference yield:

2,6-diisopropylbenzenamine (24544-04-5) → C15H27Cl2NSi2 (1309944-27-1)

Guidance literature:

Multi-step reaction with 2 steps

1.1: n-butyllithium / hexane; diethyl ether / 12 h / -78 - 20 °C / Inert atmosphere

1.2: 12 h / -78 - 20 °C / Inert atmosphere

2.1: n-butyllithium / hexane; diethyl ether / 12 h / -78 - 20 °C / Inert atmosphere

2.2: 12 h / -78 - 20 °C / Inert atmosphere

With n-butyllithium; In diethyl ether; hexane;

DOI:10.1039/c6dt00059b

Reference yield: 81.8%

C15H27Cl2NSi2 (1309944-27-1) → C30H53Cl3N2Si4 (1309944-30-6)

Guidance literature:

With 1,3-di-tert-butylimidazol-2-ylidene; In tetrahydrofuran; at -78 - 20 ℃; Inert atmosphere;

DOI:10.1002/asia.201100022

upstream raw materials:

N-trimethylsilyl-2,6-diisopropylaniline

2,6-diisopropylbenzenamine

Downstream raw materials:

C₃₀H₅₃Cl₃N₂Si₄

C₃₄H₅₅N₄Si₂

C₂₆H₄₆ClN₃Si₂

C₄₀H₅₆ClN₃Si₂