C₃₄H₃₀N₈O₆S₂

Base Information

• Chemical Name: C₃₄H₃₀N₈O₆S₂
• CAS No.: 1445860-29-6
• Molecular Formula: C₃₄H₃₀N₈O₆S₂
• Molecular Weight: 710.794

Synonyms:C₃₄H₃₀N₈O₆S₂

Chemical Property of C₃₄H₃₀N₈O₆S₂

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₃₄H₃₀N₈O₆S₂

There total 25 articles about C₃₄H₃₀N₈O₆S₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

C34H32N8O7S2 → C34H30N8O6S2 (1445860-29-6)

Guidance literature:

With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; copper(l) chloride; In dichloromethane; N,N-dimethyl-formamide; at 20 ℃; for 30h; Inert atmosphere;

DOI:10.1002/ejoc.201600994

Reference yield:

C34H32N8O6S2 → C34H30N8O6S2 (890085-24-2) + C34H30N8O6S2 (1445860-29-6)

Guidance literature:

With Bromotrichloromethane; 1,8-diazabicyclo[5.4.0]undec-7-ene; In dichloromethane; at -78 - 20 ℃; Overall yield = 1.5 mg; Inert atmosphere;

DOI:10.1021/ol401412v

Reference yield:

(N-tert-butoxycarbonyl-O-tert-butylsilyldimethoxyserinyl)serine allyl ester → C34H30N8O6S2 (1445860-29-6)

Guidance literature:

Multi-step reaction with 13 steps

1.1: diethylamino-sulfur trifluoride / dichloromethane / 3 h / -78 - 20 °C / Inert atmosphere

1.2: 0.75 h / -40 - 20 °C / Inert atmosphere

2.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / dichloromethane / 0.67 h / -55 °C / Inert atmosphere

2.2: 5 h / 20 °C / Inert atmosphere

3.1: trifluoroacetic acid / water / 14 h / 20 °C / Inert atmosphere

4.1: N-ethyl-N,N-diisopropylamine; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate / N,N-dimethyl-formamide; dichloromethane / 0.25 h / -3 °C / Inert atmosphere

4.2: 26 h / Inert atmosphere

5.1: diethylamino-sulfur trifluoride / dichloromethane / 3.5 h / -78 °C / Inert atmosphere

5.2: 2 h / -78 - 20 °C / Inert atmosphere

6.1: 1,8-diazabicyclo[5.4.0]undec-7-ene; pyridine / acetonitrile; tetrachloromethane / 72 h / -60 - 20 °C / Inert atmosphere; Darkness

7.1: trifluoroacetic acid; methoxybenzene / dichloromethane / 3 h / 0 - 20 °C / Inert atmosphere

8.1: N-ethyl-N,N-diisopropylamine; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate / dichloromethane / 0.42 h / 0 °C / Inert atmosphere

8.2: 48 h / 20 °C / Inert atmosphere

9.1: bis(dibenzylideneacetone)-palladium⁽⁰⁾; morpholine / dichloromethane / 4 h / 20 °C / Inert atmosphere

10.1: N-ethyl-N,N-diisopropylamine; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate / N,N-dimethyl-formamide; dichloromethane / 24 h / 20 °C / Inert atmosphere

11.1: triphenylphosphine; 2,6-dimethylpyridine / 7 h / 60 °C / Inert atmosphere

12.1: 1,8-diazabicyclo[5.4.0]undec-7-ene; Bromotrichloromethane / dichloromethane / 8 h / -70 - 20 °C / Inert atmosphere

13.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; copper(l) chloride / N,N-dimethyl-formamide; dichloromethane / 30 h / 20 °C / Inert atmosphere

With morpholine; pyridine; 2,6-dimethylpyridine; Bromotrichloromethane; diethylamino-sulfur trifluoride; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; methoxybenzene; 1,8-diazabicyclo[5.4.0]undec-7-ene; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; triphenylphosphine; trifluoroacetic acid; copper(l) chloride; bis(dibenzylideneacetone)-palladium⁽⁰⁾; In tetrachloromethane; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile;

DOI:10.1002/ejoc.201600994

upstream raw materials:

(2R,1'S)-(1’-((tert-butoxycarbonyl)amino)-2’-(tritylthio)ethyl)-4,5-dihydrothiazole-4-carboxylic acid methyl ester

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 1445860-29-6 C₃₄H₃₀N₈O₆S₂

Send

Send

Metric Ton KG G Pound L ML

Send

Send