3-<(1-phenylethyl)amino>propyl disulfide

Base Information

Chemical Name:3-<(1-phenylethyl)amino>propyl disulfide
CAS No.:128242-31-9
Molecular Formula:C₂₂H₃₂N₂S₂
Molecular Weight:388.641
Hs Code.:

Synonyms:3-<(1-phenylethyl)amino>propyl disulfide

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Chemical Property of 3-<(1-phenylethyl)amino>propyl disulfide

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Technology Process of 3-<(1-phenylethyl)amino>propyl disulfide

There total 3 articles about 3-<(1-phenylethyl)amino>propyl disulfide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.7%

: 4628-56-2
3-<(1-phenylethyl)amino>propanethiol

: 128242-31-9
3-<(1-phenylethyl)amino>propyl disulfide

Guidance literature:: With dihydrogen peroxide; iron(II) sulfate; In water; for 12h; Ambient temperature;
DOI:10.1021/jo00300a037

Reference yield:

: 128218-35-9
3-<(1-phenylethyl)amino>propanol

: 128242-31-9
3-<(1-phenylethyl)amino>propyl disulfide

Guidance literature:: Multi-step reaction with 2 steps

1: 1) 48percent hydrobromic acid, thiourea, 2) aqueous sodium hydroxide / 1) reflux, 12 h, 2) reflux, 4 h

2: 92.7 percent / hydrogen peroxide / ferrous sulfate / H₂O / 12 h / Ambient temperature

With sodium hydroxide; hydrogen bromide; dihydrogen peroxide; thiourea; iron(II) sulfate; In water;
DOI:10.1021/jo00300a037

Reference yield:

: 618-36-0
rac-methylbenzylamine

: 128242-31-9
3-<(1-phenylethyl)amino>propyl disulfide

Guidance literature:: Multi-step reaction with 3 steps

1: 93.2 percent / H₂O / 5.5 h / Heating

2: 1) 48percent hydrobromic acid, thiourea, 2) aqueous sodium hydroxide / 1) reflux, 12 h, 2) reflux, 4 h

3: 92.7 percent / hydrogen peroxide / ferrous sulfate / H₂O / 12 h / Ambient temperature

With sodium hydroxide; hydrogen bromide; dihydrogen peroxide; thiourea; iron(II) sulfate; In water;
DOI:10.1021/jo00300a037