5-(4-chloro-phenyl)-6-(4-methylsulfanyl-phenyl)-1-phenyl-1,5-dihydro-pyrazolo[3,4-d]pyrimidin-4-one

Base Information

Chemical Name:5-(4-chloro-phenyl)-6-(4-methylsulfanyl-phenyl)-1-phenyl-1,5-dihydro-pyrazolo[3,4-d]pyrimidin-4-one
CAS No.:954146-49-7
Molecular Formula:C₂₄H₁₇ClN₄OS
Molecular Weight:444.944
Hs Code.:

Synonyms:5-(4-chloro-phenyl)-6-(4-methylsulfanyl-phenyl)-1-phenyl-1,5-dihydro-pyrazolo[3,4-d]pyrimidin-4-one

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Chemical Property of 5-(4-chloro-phenyl)-6-(4-methylsulfanyl-phenyl)-1-phenyl-1,5-dihydro-pyrazolo[3,4-d]pyrimidin-4-one

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Technology Process of 5-(4-chloro-phenyl)-6-(4-methylsulfanyl-phenyl)-1-phenyl-1,5-dihydro-pyrazolo[3,4-d]pyrimidin-4-one

There total 1 articles about 5-(4-chloro-phenyl)-6-(4-methylsulfanyl-phenyl)-1-phenyl-1,5-dihydro-pyrazolo[3,4-d]pyrimidin-4-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 402771-57-7
6-(4-bromo-phenyl)-5-(4-chloro-phenyl)-1-phenyl-1,5-dihydro-pyrazolo[3,4-d]pyrimidin-4-one

: 5188-07-8
sodium thiomethoxide

: 954146-49-7
5-(4-chloro-phenyl)-6-(4-methylsulfanyl-phenyl)-1-phenyl-1,5-dihydro-pyrazolo[3,4-d]pyrimidin-4-one

Guidance literature:: In N,N-dimethyl-formamide; at 80 ℃; for 1.5h;

Reference yield:

: 954146-49-7
5-(4-chloro-phenyl)-6-(4-methylsulfanyl-phenyl)-1-phenyl-1,5-dihydro-pyrazolo[3,4-d]pyrimidin-4-one

: 954146-50-0
5-(4-chloro-phenyl)-6-(4-methanesulfinyl-phenyl)-1-phenyl-1,5-dihydro-pyrazolo[3,4-d]pyrimidin-4-one

Guidance literature:: With Monoperoxyphthalic acid, magnesium salt; In methanol; dichloromethane; at 0 ℃; for 3h;

Reference yield:

: 954146-49-7
5-(4-chloro-phenyl)-6-(4-methylsulfanyl-phenyl)-1-phenyl-1,5-dihydro-pyrazolo[3,4-d]pyrimidin-4-one

: 954145-66-5
4-[5-(4-chloro-phenyl)-4-oxo-1-phenyl-4,5-dihydro-1H-pyrazolo[3,4-d]pyrimidin-6-yl]-benzenesulfonamide

Guidance literature:: Multi-step reaction with 4 steps

1.1: Monoperoxyphthalic acid, magnesium salt / methanol; dichloromethane / 3 h / 0 °C

2.1: sodium acetate / 5 h / Heating / reflux

3.1: Monoperoxyphthalic acid, magnesium salt / methanol; dichloromethane / 18 h / 0 - 20 °C

4.1: methanol; sodium acetate / 0.25 h / 20 °C

4.2: 1.5 h

4.3: 2 h

With methanol; sodium acetate; Monoperoxyphthalic acid, magnesium salt; In methanol; dichloromethane;