Technology Process of C19H25N3O6
There total 5 articles about C19H25N3O6 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
lithium hydroxide monohydrate;
In
tetrahydrofuran; water;
at 0 ℃;
for 1h;
Inert atmosphere;
DOI:10.1002/chem.201200457
- Guidance literature:
-
Multi-step reaction with 4 steps
1: N-ethyl-N,N-diisopropylamine / isopropyl alcohol / 5 h / 20 °C / Inert atmosphere
2: palladium on activated charcoal; hydrogen / tetrahydrofuran / 4 h / 20 °C / Inert atmosphere
3: tetrahydrofuran / 20 °C / Inert atmosphere
4: lithium hydroxide monohydrate / tetrahydrofuran; water / 1 h / 0 °C / Inert atmosphere
With
lithium hydroxide monohydrate; palladium on activated charcoal; hydrogen; N-ethyl-N,N-diisopropylamine;
In
tetrahydrofuran; water; isopropyl alcohol;
DOI:10.1002/chem.201200457
- Guidance literature:
-
Multi-step reaction with 5 steps
1: triethylsilane / dichloromethane / 2 h / 20 °C / Inert atmosphere
2: N-ethyl-N,N-diisopropylamine / isopropyl alcohol / 5 h / 20 °C / Inert atmosphere
3: palladium on activated charcoal; hydrogen / tetrahydrofuran / 4 h / 20 °C / Inert atmosphere
4: tetrahydrofuran / 20 °C / Inert atmosphere
5: lithium hydroxide monohydrate / tetrahydrofuran; water / 1 h / 0 °C / Inert atmosphere
With
triethylsilane; lithium hydroxide monohydrate; palladium on activated charcoal; hydrogen; N-ethyl-N,N-diisopropylamine;
In
tetrahydrofuran; dichloromethane; water; isopropyl alcohol;
DOI:10.1002/chem.201200457