1,2-dibenzoyl-1',2',3',4',5'-pentamethylrhodocenium chloride

Base Information

Chemical Name:1,2-dibenzoyl-1',2',3',4',5'-pentamethylrhodocenium chloride
CAS No.:1315085-42-7
Molecular Formula:C₂₉H₂₈O₂Rh*Cl
Molecular Weight:546.899
Hs Code.:

Synonyms:1,2-dibenzoyl-1',2',3',4',5'-pentamethylrhodocenium chloride

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,2-dibenzoyl-1',2',3',4',5'-pentamethylrhodocenium chloride

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Technology Process of 1,2-dibenzoyl-1',2',3',4',5'-pentamethylrhodocenium chloride

There total 1 articles about 1,2-dibenzoyl-1',2',3',4',5'-pentamethylrhodocenium chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer

: 73675-12-4
2-benzoyl-6-hydroxy-6-phenylpentafulvalene

: 1315085-42-7
1,2-dibenzoyl-1',2',3',4',5'-pentamethylrhodocenium chloride

Guidance literature:: With KH; In tetrahydrofuran; byproducts: H2; (Ar), pentafulvene in dry THF cooled to 0°C, treated with excess KH, stirred, warmed to room temp., stirred overnight, filtered, treated with Rh complex (0.5 equiv.), stirred at room temp. for 4 d; evapd.(vac.), exposed to air, hydrolized (H2O), extd.(CH2Cl2), org. layer dried (brine with Na2SO4), evapd.(vac.), chromy.(silica - CH2Cl2, CH3OH), evapd., elem. anal.;
DOI:10.1002/ejic.201100226