cyclo<-L-Phenylalanyl-D-prolyl-L-phenylalanyl-L-alanyl-O-(2',3',4',6'-tetra-O-acetyl-β-D-galactopyranosyl)-(1-4)-(3,6-di-O-acetyl-2-desoxy-α-D-arabino-hexopyranosyl)-(1-6)-L-(2-amino-6-hydroxy)caproyl-L-phenylalanyl->

Base Information

Chemical Name:cyclo<-L-Phenylalanyl-D-prolyl-L-phenylalanyl-L-alanyl-O-(2',3',4',6'-tetra-O-acetyl-β-D-galactopyranosyl)-(1-4)-(3,6-di-O-acetyl-2-desoxy-α-D-arabino-hexopyranosyl)-(1-6)-L-(2-amino-6-hydroxy)caproyl-L-phenylalanyl->
CAS No.:134262-50-3
Molecular Formula:C₆₅H₈₂N₆O₂₂
Molecular Weight:1299.39
Hs Code.:

cyclo<-L-Phenylalanyl-D-prolyl-L-phenylalanyl-L-alanyl-O-(2',3',4',6'-tetra-O-acetyl-β-D-galactopyranosyl)-(1-4)-(3,6-di-O-acetyl-2-desoxy-α-D-arabino-hexopyranosyl)-(1-6)-L-(2-amino-6-hydroxy)caproyl-L-phenylalanyl->

Synonyms:cyclo<-L-Phenylalanyl-D-prolyl-L-phenylalanyl-L-alanyl-O-(2',3',4',6'-tetra-O-acetyl-β-D-galactopyranosyl)-(1-4)-(3,6-di-O-acetyl-2-desoxy-α-D-arabino-hexopyranosyl)-(1-6)-L-(2-amino-6-hydroxy)caproyl-L-phenylalanyl->

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Chemical Property of cyclo<-L-Phenylalanyl-D-prolyl-L-phenylalanyl-L-alanyl-O-(2',3',4',6'-tetra-O-acetyl-β-D-galactopyranosyl)-(1-4)-(3,6-di-O-acetyl-2-desoxy-α-D-arabino-hexopyranosyl)-(1-6)-L-(2-amino-6-hydroxy)caproyl-L-phenylalanyl->

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Technology Process of cyclo<-L-Phenylalanyl-D-prolyl-L-phenylalanyl-L-alanyl-O-(2',3',4',6'-tetra-O-acetyl-β-D-galactopyranosyl)-(1-4)-(3,6-di-O-acetyl-2-desoxy-α-D-arabino-hexopyranosyl)-(1-6)-L-(2-amino-6-hydroxy)caproyl-L-phenylalanyl->

There total 3 articles about cyclo<-L-Phenylalanyl-D-prolyl-L-phenylalanyl-L-alanyl-O-(2',3',4',6'-tetra-O-acetyl-β-D-galactopyranosyl)-(1-4)-(3,6-di-O-acetyl-2-desoxy-α-D-arabino-hexopyranosyl)-(1-6)-L-(2-amino-6-hydroxy)caproyl-L-phenylalanyl-> which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 134262-47-8
cyclo<-L-Phenylalanyl-D-prolyl-L-phenylalanyl-L-alanyl-O-(2',3',4',6'-tetra-O-acetyl-β-D-galactopyranosyl)-(1-4)-O-(3,6-di-O-acetyl-2-desoxy-2-iod-α-D-mannopyranosyl)-(1-6)-L-(2-amino-6-hydroxy)caproyl-L-phenylalanyl->

: 134262-50-3
cyclo<-L-Phenylalanyl-D-prolyl-L-phenylalanyl-L-alanyl-O-(2',3',4',6'-tetra-O-acetyl-β-D-galactopyranosyl)-(1-4)-(3,6-di-O-acetyl-2-desoxy-α-D-arabino-hexopyranosyl)-(1-6)-L-(2-amino-6-hydroxy)caproyl-L-phenylalanyl->

Guidance literature:: With hydrogen; nickel; In ethanol; for 7h; Ambient temperature; other condition: NiCl₂*6H₂O, H₃BO₃, NaBH₄, EtOH, CH₂Cl₂, 2 h, room temperature;

Reference yield:

: 51450-24-9
hexa-O-acetyl-D-lactal

: 134262-50-3
cyclo<-L-Phenylalanyl-D-prolyl-L-phenylalanyl-L-alanyl-O-(2',3',4',6'-tetra-O-acetyl-β-D-galactopyranosyl)-(1-4)-(3,6-di-O-acetyl-2-desoxy-α-D-arabino-hexopyranosyl)-(1-6)-L-(2-amino-6-hydroxy)caproyl-L-phenylalanyl->

Guidance literature:: Multi-step reaction with 2 steps

1: 67 percent / N-iodosuccinimide / acetonitrile / 144 h / 40 °C

2: 86 percent / H₂ / Raney-nickel / aq. ethanol / 7 h / Ambient temperature; other condition: NiCl₂*6H₂O, H₃BO₃, NaBH₄, EtOH, CH₂Cl₂, 2 h, room temperature

With N-iodo-succinimide; hydrogen; nickel; In ethanol; acetonitrile;

Reference yield:

: 134262-59-2
cyclo<-Phe-D-Pro-Phe-Ala-Ahc-Phe->

: 134262-50-3
cyclo<-L-Phenylalanyl-D-prolyl-L-phenylalanyl-L-alanyl-O-(2',3',4',6'-tetra-O-acetyl-β-D-galactopyranosyl)-(1-4)-(3,6-di-O-acetyl-2-desoxy-α-D-arabino-hexopyranosyl)-(1-6)-L-(2-amino-6-hydroxy)caproyl-L-phenylalanyl->

Guidance literature:: Multi-step reaction with 2 steps

1: 67 percent / N-iodosuccinimide / acetonitrile / 144 h / 40 °C

2: 86 percent / H₂ / Raney-nickel / aq. ethanol / 7 h / Ambient temperature; other condition: NiCl₂*6H₂O, H₃BO₃, NaBH₄, EtOH, CH₂Cl₂, 2 h, room temperature

With N-iodo-succinimide; hydrogen; nickel; In ethanol; acetonitrile;