1-[2-((S)-1-hydroxy-2-phenyl-2-ethanylamino)-2-oxoethyl]-3-methylbenzimidazolium chloride

Base Information

Chemical Name:1-[2-((S)-1-hydroxy-2-phenyl-2-ethanylamino)-2-oxoethyl]-3-methylbenzimidazolium chloride
CAS No.:1204985-23-8
Molecular Formula:C₁₈H₂₀N₃O₂*Cl
Molecular Weight:345.829
Hs Code.:

Synonyms:1-[2-((S)-1-hydroxy-2-phenyl-2-ethanylamino)-2-oxoethyl]-3-methylbenzimidazolium chloride

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Chemical Property of 1-[2-((S)-1-hydroxy-2-phenyl-2-ethanylamino)-2-oxoethyl]-3-methylbenzimidazolium chloride

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Technology Process of 1-[2-((S)-1-hydroxy-2-phenyl-2-ethanylamino)-2-oxoethyl]-3-methylbenzimidazolium chloride

There total 1 articles about 1-[2-((S)-1-hydroxy-2-phenyl-2-ethanylamino)-2-oxoethyl]-3-methylbenzimidazolium chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 1632-83-3
1-Methylbenzimidazole

: 291545-74-9
(S)-2-chloro-N-(2-hydroxyl-1-phenylethyl)acetamide

: 1204985-23-8
1-[2-((S)-1-hydroxy-2-phenyl-2-ethanylamino)-2-oxoethyl]-3-methylbenzimidazolium chloride

Guidance literature:: In 1,4-dioxane; at 110 ℃; for 16h;
DOI:10.1016/j.jorganchem.2009.10.011

Reference yield: 52.0%

: 21264-30-2,90243-59-7,14592-56-4
dichloro bis(acetonitrile) palladium(II)

: 1204985-23-8
1-[2-((S)-1-hydroxy-2-phenyl-2-ethanylamino)-2-oxoethyl]-3-methylbenzimidazolium chloride

: 20667-12-3
silver(l) oxide

: 1-[2-((S)-1-hydroxy-2-phenyl-2-ethanylamino)-2-oxoethyl]-3-methylbenzimidazolium palladium chloride

Guidance literature:: In CH₂Cl₂; acetonitrile; byproducts: HCl; suspension of azolium compd. and Ag2O in CH2Cl2 stirred for 2 h in dark at refluxing temp.; concd. under reduced pressure; Pd complex added to suspn. of Ag complex in MeCN in the dark at room temp.; stirred for 2 h; filtered through plug of glass fiber filter paper; evapd. to dryness in vacuo, crystd. from ethyl acetate or MeOH; elem. anal.;
DOI:10.1016/j.jorganchem.2009.10.011

Reference yield:

: 21264-30-2,90243-59-7,14592-56-4
dichloro bis(acetonitrile) palladium(II)

: 1204985-23-8
1-[2-((S)-1-hydroxy-2-phenyl-2-ethanylamino)-2-oxoethyl]-3-methylbenzimidazolium chloride

: 1-[2-((S)-1-hydroxy-2-phenyl-2-ethanylamino)-2-oxoethyl]-3-methylbenzimidazolium palladium chloride

Guidance literature:: 1-[2-((S)-1-hydroxy-2-phenyl-2-ethanylamino)-2-oxoethyl]-3-methylbenzimidazolium chloride; With silver(l) oxide; In dichloromethane; for 2h; Darkness; Reflux;

dichloro bis(acetonitrile) palladium(II); In acetonitrile; at 20 ℃; for 2h; Darkness;
DOI:10.1016/j.jorganchem.2012.12.015