Technology Process of C27H28N4O8
There total 6 articles about C27H28N4O8 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
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Multi-step reaction with 6 steps
1.1: N-ethyl-N,N-diisopropylamine / chloroform / 1 h / 0 - 20 °C
2.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / tetrahydrofuran; water / 1 h / 20 °C
3.1: trifluoroacetic acid; thallium(III) trifluoroacetate / 1 h / 20 °C
3.2: 0.17 h / 140 °C
4.1: sodium tetrahydroborate; boron trifluoride diethyl etherate / tetrahydrofuran / 1 h / 20 °C
5.1: potassium nitrosodisulfonate / water; acetone / 20 °C / pH 7.2 / Aqueous phosphate buffer
6.1: methanol / 12 h / 20 °C
With
sodium tetrahydroborate; potassium nitrosodisulfonate; boron trifluoride diethyl etherate; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; 2,3-dicyano-5,6-dichloro-p-benzoquinone; thallium(III) trifluoroacetate;
In
tetrahydrofuran; methanol; chloroform; water; acetone;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: potassium nitrosodisulfonate / water; acetone / 20 °C / pH 7.2 / Aqueous phosphate buffer
2: methanol / 12 h / 20 °C
With
potassium nitrosodisulfonate;
In
methanol; water; acetone;