2-[5-Chloro-4-methyl-2-(2-oxo-imidazolidine-1-sulfonyl)-phenylsulfanyl]-octanoic acid

Base Information

Chemical Name:2-[5-Chloro-4-methyl-2-(2-oxo-imidazolidine-1-sulfonyl)-phenylsulfanyl]-octanoic acid
CAS No.:168698-66-6
Molecular Formula:C₁₈H₂₅ClN₂O₅S₂
Molecular Weight:448.992
Hs Code.:

Synonyms:2-[5-Chloro-4-methyl-2-(2-oxo-imidazolidine-1-sulfonyl)-phenylsulfanyl]-octanoic acid

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Chemical Property of 2-[5-Chloro-4-methyl-2-(2-oxo-imidazolidine-1-sulfonyl)-phenylsulfanyl]-octanoic acid

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Technology Process of 2-[5-Chloro-4-methyl-2-(2-oxo-imidazolidine-1-sulfonyl)-phenylsulfanyl]-octanoic acid

There total 1 articles about 2-[5-Chloro-4-methyl-2-(2-oxo-imidazolidine-1-sulfonyl)-phenylsulfanyl]-octanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 2623-82-7,70610-87-6
2-bromooctanoic acid

: 114436-08-7
1-(4-chloro-2-mercapto-5-methylbenzenesulfonyl)imidazolidin-2-one

: 168698-66-6
2-[5-Chloro-4-methyl-2-(2-oxo-imidazolidine-1-sulfonyl)-phenylsulfanyl]-octanoic acid

Guidance literature:: With sodium hydroxide; sodium carbonate; In water; at 40 - 80 ℃; for 6.5h;

Reference yield:

: 168698-66-6
2-[5-Chloro-4-methyl-2-(2-oxo-imidazolidine-1-sulfonyl)-phenylsulfanyl]-octanoic acid

: 2-[5-Chloro-4-methyl-2-(2-oxo-imidazolidine-1-sulfonyl)-phenylsulfanyl]-octanoic acid (2-dimethylamino-ethyl)-amide

Guidance literature:: Multi-step reaction with 2 steps

1: thionyl chloride / 3 h / Heating

2: benzene / 40 h / 15 - 20 °C

With thionyl chloride; In benzene;

Reference yield:

: 168698-66-6
2-[5-Chloro-4-methyl-2-(2-oxo-imidazolidine-1-sulfonyl)-phenylsulfanyl]-octanoic acid

: 2-[5-Chloro-4-methyl-2-(2-oxo-imidazolidine-1-sulfonyl)-phenylsulfanyl]-octanoic acid (2-diethylamino-ethyl)-amide

Guidance literature:: Multi-step reaction with 2 steps

1: thionyl chloride / 3 h / Heating

2: benzene / 40 h / 15 - 20 °C

With thionyl chloride; In benzene;