4-chloro-12-phenylcarbonyloxy-3,5,8,10,13-pentaoxa-4-phosphatetracyclo[7.3.1.0^2,7.0^6,11]tridecane

Base Information

• Chemical Name: 4-chloro-12-phenylcarbonyloxy-3,5,8,10,13-pentaoxa-4-phosphatetracyclo[7.3.1.0^2,7.0^6,11]tridecane
• CAS No.: 943139-86-4
• Molecular Formula: C₁₄H₁₂ClO₇P
• Molecular Weight: 358.672

Synonyms:4-chloro-12-phenylcarbonyloxy-3,5,8,10,13-pentaoxa-4-phosphatetracyclo[7.3.1.0^2,7.0^6,11]tridecane

Chemical Property of 4-chloro-12-phenylcarbonyloxy-3,5,8,10,13-pentaoxa-4-phosphatetracyclo[7.3.1.0^2,7.0^6,11]tridecane

Chemical Property:

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Technology Process of 4-chloro-12-phenylcarbonyloxy-3,5,8,10,13-pentaoxa-4-phosphatetracyclo[7.3.1.0^2,7.0^6,11]tridecane

There total 1 articles about 4-chloro-12-phenylcarbonyloxy-3,5,8,10,13-pentaoxa-4-phosphatetracyclo[7.3.1.0^2,7.0^6,11]tridecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

8,9-dihydroxy-6-phenylcarbonyloxy-2,4,10-trioxa-tricyclo[3.3.1.13,7]decane → 4-chloro-12-phenylcarbonyloxy-3,5,8,10,13-pentaoxa-4-phosphatetracyclo[7.3.1.02,7.06,11]tridecane (943139-86-4)

Guidance literature:

With phosphorus trichloride; for 24h; Heating;

DOI:10.1016/j.carres.2007.02.031

Reference yield: 82.0%

4-chloro-12-phenylcarbonyloxy-3,5,8,10,13-pentaoxa-4-phosphatetracyclo[7.3.1.02,7.06,11]tridecane (943139-86-4) + isopropylamine (75-31-0) → 4-isopropylamino-12-phenylcarbonyloxy-3,5,8,10,13-pentaoxa-4-phosphatetracyclo[7.3.1.02,7.06,11]tridecane

Guidance literature:

In toluene; at 25 ℃; for 12h;

DOI:10.1016/j.carres.2007.02.031

Reference yield:

4-chloro-12-phenylcarbonyloxy-3,5,8,10,13-pentaoxa-4-phosphatetracyclo[7.3.1.02,7.06,11]tridecane (943139-86-4) → C23H20Cl4NO9P

Guidance literature:

Multi-step reaction with 2 steps

1: 82 percent / toluene / 12 h / 25 °C

2: 70 percent / toluene

In toluene;

DOI:10.1016/j.carres.2007.02.031

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