C₃₈H₅₄O₈Si

Base Information

Chemical Name:C₃₈H₅₄O₈Si
CAS No.:782479-09-8
Molecular Formula:C₃₈H₅₄O₈Si
Molecular Weight:666.927
Hs Code.:

C<sub>38</sub>H<sub>54</sub>O<sub>8</sub>Si

Synonyms:C₃₈H₅₄O₈Si

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Chemical Property of C₃₈H₅₄O₈Si

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Technology Process of C₃₈H₅₄O₈Si

There total 26 articles about C₃₈H₅₄O₈Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 782479-32-7
C₃₈H₅₂O₈Si

: 782479-09-8
C₃₈H₅₄O₈Si

Guidance literature:: With sodium tetrahydroborate; In methanol; at -5 ℃; for 0.0833333h;
DOI:10.1021/ja054750q

Reference yield:

: 782479-31-6
C₄₁H₅₈O₇S₂Si

: 782479-09-8
C₃₈H₅₄O₈Si

Guidance literature:: C₄₁H₅₈O₇S₂Si; With 2,6-dimethylpyridine; N-Bromosuccinimide; In water; acetonitrile; at 25 ℃; for 1h;

With sodium tetrahydroborate; In methanol; at -78 - -60 ℃; for 3h;
DOI:10.1002/anie.200460696

Reference yield:

: 881651-51-0
(2S,3R,5S)-2-((1S,2R)-3-Benzyloxy-1-iodo-2-methyl-propyl)-3-(tert-butyl-dimethyl-silanyloxy)-5-(tert-butyl-diphenyl-silanyloxymethyl)-tetrahydro-furan

: 782479-09-8
C₃₈H₅₄O₈Si

Guidance literature:: Multi-step reaction with 17 steps

1.1: 99 percent / H₂ / Raney-Ni / ethanol / 1 h / 25 °C

2.1: 88 percent / H₂ / Pd(OH)2/C / ethanol / 3 h / 25 °C

3.1: 99 percent / Dess-Martin periodinane / CH₂Cl₂ / 2 h / 0 - 25 °C

4.1: Mg / tetrahydrofuran / 2 h / 25 °C

4.2: tetrahydrofuran / 2 h / -78 - 0 °C

5.1: 40.9 g / Dess-Martin periodinane / CH₂Cl₂ / 4 h / 0 - 25 °C

6.1: 98 percent / triethyl orthoformate; p-TsOH / 2.5 h / 55 °C

7.1: 96 percent / TBAF / tetrahydrofuran / 48 h / 25 °C

8.1: 97 percent / Et₃N; 4-DMAP / CH₂Cl₂ / 16 h / 0 - 25 °C

9.1: 98 percent / imidazole; 4-DMAP / CH₂Cl₂ / 0.5 h / 0 °C

10.1: N-methylmorpholine-N-oxide; OsO₄ / 2-methyl-propan-2-ol; H₂O; tetrahydrofuran / 12 h / 25 °C

11.1: 41.5 g / NaIO₄ / 2-methyl-propan-2-ol; H₂O; various solvents / 5 h / 20 °C / pH 7

12.1: n-BuLi / toluene; tetrahydrofuran / 3 h / -30 °C

12.2: tetrahydrofuran; toluene / 1 h / -30 °C

13.1: 13.2 g / Dess-Martin periodinane; pyridine / CH₂Cl₂ / 2 h / 0 °C

14.1: 70 percent / TMSOTf / CH₂Cl₂ / 3 h / -78 - -30 °C

15.1: 95 percent / 4-DMAP; pyridine / CH₂Cl₂ / 3 h / 0 - 25 °C

16.1: 91 percent / 2,6-lutidine; N-bromosuccinimide; H₂O / acetonitrile / 2 h / 25 °C

17.1: 92 percent / NaBH₄ / methanol / 0.08 h / -5 °C

With pyridine; 1H-imidazole; 2,6-dimethylpyridine; dmap; sodium tetrahydroborate; sodium periodate; N-Bromosuccinimide; osmium(VIII) oxide; n-butyllithium; trimethylsilyl trifluoromethanesulfonate; tetrabutyl ammonium fluoride; water; hydrogen; Dess-Martin periodane; toluene-4-sulfonic acid; magnesium; 4-methylmorpholine N-oxide; triethylamine; orthoformic acid triethyl ester; palladium dihydroxide; nickel; In tetrahydrofuran; methanol; ethanol; dichloromethane; various solvents; water; toluene; acetonitrile; tert-butyl alcohol;
DOI:10.1021/ja054750q