Phenyl-phosphonic acid mono-[2-(3,3,10,10-tetramethyl-[1,2,5,8]dithiadiazecan-5-yl)-ethyl] ester

Base Information

Chemical Name:Phenyl-phosphonic acid mono-[2-(3,3,10,10-tetramethyl-[1,2,5,8]dithiadiazecan-5-yl)-ethyl] ester
CAS No.:212774-78-2
Molecular Formula:C₁₈H₃₁N₂O₃PS₂
Molecular Weight:418.561
Hs Code.:

Synonyms:Phenyl-phosphonic acid mono-[2-(3,3,10,10-tetramethyl-[1,2,5,8]dithiadiazecan-5-yl)-ethyl] ester

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Chemical Property of Phenyl-phosphonic acid mono-[2-(3,3,10,10-tetramethyl-[1,2,5,8]dithiadiazecan-5-yl)-ethyl] ester

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Technology Process of Phenyl-phosphonic acid mono-[2-(3,3,10,10-tetramethyl-[1,2,5,8]dithiadiazecan-5-yl)-ethyl] ester

There total 3 articles about Phenyl-phosphonic acid mono-[2-(3,3,10,10-tetramethyl-[1,2,5,8]dithiadiazecan-5-yl)-ethyl] ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 824-72-6
P,P-dichlorophenylphosphine oxide

: 142991-44-4
5-(2-hydroxyethyl)-3,3,10,10-tetramethyl-1,2-dithia-5,8-diazacyclodecane

: 212774-78-2
Phenyl-phosphonic acid mono-[2-(3,3,10,10-tetramethyl-[1,2,5,8]dithiadiazecan-5-yl)-ethyl] ester

Guidance literature:: With pyridine; at 0 ℃; for 1h;
DOI:10.1080/00304949809355318

Reference yield:

: 108168-04-3
6,6,9,9-tetramethylhexahydroimidazo[2,1-d][1,2,5]dithiazepine

: 212774-78-2
Phenyl-phosphonic acid mono-[2-(3,3,10,10-tetramethyl-[1,2,5,8]dithiadiazecan-5-yl)-ethyl] ester

Guidance literature:: Multi-step reaction with 3 steps

1: 65 percent / Na₂CO₃, NaI / ethanol / 16 h / Heating

2: 48 percent / NaBH₄, AcOH / 2 h / Ambient temperature

3: 80 percent / pyridine / 1 h / 0 °C

With pyridine; sodium tetrahydroborate; sodium carbonate; acetic acid; sodium iodide; In ethanol;
DOI:10.1080/00304949809355318

Reference yield:

: 142991-41-1
2-(6,6,9,9-Tetramethyl-hexahydro-imidazo[2,1-d][1,2,5]dithiazepin-1-yl)-ethanol

: 212774-78-2
Phenyl-phosphonic acid mono-[2-(3,3,10,10-tetramethyl-[1,2,5,8]dithiadiazecan-5-yl)-ethyl] ester

Guidance literature:: Multi-step reaction with 2 steps

1: 48 percent / NaBH₄, AcOH / 2 h / Ambient temperature

2: 80 percent / pyridine / 1 h / 0 °C

With pyridine; sodium tetrahydroborate; acetic acid;
DOI:10.1080/00304949809355318