Tetraisopropylazodicarboxamid

Base Information

• Chemical Name: Tetraisopropylazodicarboxamid
• CAS No.: 155877-06-8
• Molecular Formula: C₁₄H₂₈N₄O₂
• Molecular Weight: 284.402
• European Community (EC) Number: 605-030-3
• Mol file: 155877-06-8.mol

Synonyms:Tetraisopropylazodicarboxamid;tetraisopropylazodicarboxamide;155877-06-8;(3E)-3-[di(propan-2-yl)carbamoylimino]-1,1-di(propan-2-yl)urea;SCHEMBL103044;CS-0276227;N1,N1,N2,N2-Tetraisopropyldiazene-1,2-dicarboxamide

Chemical Property of Tetraisopropylazodicarboxamid

Chemical Property:

• Boiling Point: 341.2±25.0 °C(Predicted)
• PKA: -0.76±0.70(Predicted)
• PSA: 65.34000
• Density: 1.02±0.1 g/cm3(Predicted)
• LogP: 3.91620
• XLogP3: 3.4
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 4
• Exact Mass: 284.22122615
• Heavy Atom Count: 20
• Complexity: 312

Purity/Quality:

99.0% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC(C)N(C(C)C)C(=O)N=NC(=O)N(C(C)C)C(C)C
• Isomeric SMILES: CC(C)N(C(C)C)C(=O)/N=N/C(=O)N(C(C)C)C(C)C

Technology Process of Tetraisopropylazodicarboxamid

There total 2 articles about Tetraisopropylazodicarboxamid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

C14H30N4O2 → N,N,N',N'-tetraisopropylazodicarboxamide (155877-06-8)

Guidance literature:

With pyridine; N-Bromosuccinimide; Ambient temperature;

DOI:10.1246/cl.1994.539

Reference yield:

diisopropylamine (108-18-9) → N,N,N',N'-tetraisopropylazodicarboxamide (155877-06-8)

Guidance literature:

Multi-step reaction with 2 steps

1: 56 percent / CHCl₃ / Heating

2: 100 percent / NBS, pyridine / Ambient temperature

With pyridine; N-Bromosuccinimide; In chloroform;

DOI:10.1246/cl.1994.539

upstream raw materials:

diisopropylamine

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