N,N,N',N'-tetrakis(2-ethylhexyl)-5-trimethylsilylethynylisophthalamide

Base Information

Chemical Name:N,N,N',N'-tetrakis(2-ethylhexyl)-5-trimethylsilylethynylisophthalamide
CAS No.:338949-07-8
Molecular Formula:C₄₅H₈₀N₂O₂Si
Molecular Weight:709.228
Hs Code.:

Synonyms:N,N,N',N'-tetrakis(2-ethylhexyl)-5-trimethylsilylethynylisophthalamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N,N,N',N'-tetrakis(2-ethylhexyl)-5-trimethylsilylethynylisophthalamide

Chemical Property:

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Technology Process of N,N,N',N'-tetrakis(2-ethylhexyl)-5-trimethylsilylethynylisophthalamide

There total 3 articles about N,N,N',N'-tetrakis(2-ethylhexyl)-5-trimethylsilylethynylisophthalamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 338949-06-7
N,N,N',N'-tetrakis(2-ethylhexyl)-5-iodoisophthalamide

: 1066-54-2
trimethylsilylacetylene

: 338949-07-8
N,N,N',N'-tetrakis(2-ethylhexyl)-5-trimethylsilylethynylisophthalamide

Guidance literature:: With palladium diacetate; copper(l) iodide; triphenylphosphine; at 50 ℃; for 1h;
DOI:10.1039/b007250h

Reference yield:

: 51839-16-8
5-iodoisophthalic acid

: 338949-07-8
N,N,N',N'-tetrakis(2-ethylhexyl)-5-trimethylsilylethynylisophthalamide

Guidance literature:: Multi-step reaction with 3 steps

1: SOCl₂ / 16 h / Heating

2: 7.63 g / Et₃N / toluene / 20 °C

3: 89 percent / Pd(OAc)2; PPh₃; CuI / 1 h / 50 °C

With palladium diacetate; copper(l) iodide; thionyl chloride; triethylamine; triphenylphosphine; In toluene;
DOI:10.1039/b007250h

Reference yield:

: 175791-94-3
5-iodoisophthalic acid dichloride

: 338949-07-8
N,N,N',N'-tetrakis(2-ethylhexyl)-5-trimethylsilylethynylisophthalamide

Guidance literature:: Multi-step reaction with 2 steps

1: 7.63 g / Et₃N / toluene / 20 °C

2: 89 percent / Pd(OAc)2; PPh₃; CuI / 1 h / 50 °C

With palladium diacetate; copper(l) iodide; triethylamine; triphenylphosphine; In toluene;
DOI:10.1039/b007250h