(+/-)-α-[[2-(1H-pyrrol-1-yl)phenyl]thio]-p-tolylacetic acid ethyl ester

Base Information

Chemical Name:(+/-)-α-[[2-(1H-pyrrol-1-yl)phenyl]thio]-p-tolylacetic acid ethyl ester
CAS No.:1268473-56-8
Molecular Formula:C₂₁H₂₁NO₂S
Molecular Weight:351.469
Hs Code.:

Synonyms:(+/-)-α-[[2-(1H-pyrrol-1-yl)phenyl]thio]-p-tolylacetic acid ethyl ester

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Chemical Property of (+/-)-α-[[2-(1H-pyrrol-1-yl)phenyl]thio]-p-tolylacetic acid ethyl ester

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Technology Process of (+/-)-α-[[2-(1H-pyrrol-1-yl)phenyl]thio]-p-tolylacetic acid ethyl ester

There total 1 articles about (+/-)-α-[[2-(1H-pyrrol-1-yl)phenyl]thio]-p-tolylacetic acid ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 43153-75-9
bis(2-N-pyrrolylphenyl) disulfide

: 15674-78-9
(+/-)-α-bromo-p-tolylacetic acid ethyl ester

: 1268473-56-8
(+/-)-α-[[2-(1H-pyrrol-1-yl)phenyl]thio]-p-tolylacetic acid ethyl ester

Guidance literature:: bis(2-N-pyrrolylphenyl) disulfide; With sodium tetrahydroborate; In ethanol; for 0.5h; Inert atmosphere; Reflux;

(+/-)-α-bromo-p-tolylacetic acid ethyl ester; In ethanol; at 20 ℃; for 8h; Inert atmosphere;
DOI:10.1021/jm101438u

Reference yield:

: 1268473-56-8
(+/-)-α-[[2-(1H-pyrrol-1-yl)phenyl]thio]-p-tolylacetic acid ethyl ester

: 1268473-57-9
(+/-)-α-[[2-(1H-pyrrol-1-yl)phenyl]thio]-p-tolylacetic Acid

Guidance literature:: With water; sodium hydroxide; In tetrahydrofuran; ethanol; at 20 ℃; for 12h;
DOI:10.1021/jm101438u

Reference yield:

: 1268473-56-8
(+/-)-α-[[2-(1H-pyrrol-1-yl)phenyl]thio]-p-tolylacetic acid ethyl ester

: 1268473-58-0
(+/-)-6-(p-tolyl)pyrrolo[2,1-d][1,5]benzothiazepin-7-(6H)-one

Guidance literature:: Multi-step reaction with 2 steps

1: water; sodium hydroxide / tetrahydrofuran; ethanol / 12 h / 20 °C

2: phosphorus pentachloride / dichloromethane / 7 h / Reflux

With phosphorus pentachloride; water; sodium hydroxide; In tetrahydrofuran; ethanol; dichloromethane;
DOI:10.1021/jm101438u