C₁₁H₁₂ClFO₄S

Base Information

Chemical Name:C₁₁H₁₂ClFO₄S
CAS No.:1402742-04-4
Molecular Formula:C₁₁H₁₂ClFO₄S
Molecular Weight:294.731
Hs Code.:

C<sub>11</sub>H<sub>12</sub>ClFO<sub>4</sub>S

Synonyms:C₁₁H₁₂ClFO₄S

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₁H₁₂ClFO₄S

Chemical Property:

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Technology Process of C₁₁H₁₂ClFO₄S

There total 2 articles about C₁₁H₁₂ClFO₄S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1402742-03-3
C₁₁H₁₃FO₅S

: 1402742-04-4
C₁₁H₁₂ClFO₄S

Guidance literature:: With thionyl chloride; for 3h; Reflux;

Reference yield:

: 1259524-13-4
ethyl 2-(2-fluorophenyl)acrylate

: 1402742-04-4
C₁₁H₁₂ClFO₄S

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydrogensulfite / ethanol; water / 0.5 h / 165 °C / microwave reactor

2: thionyl chloride / 3 h / Reflux

With thionyl chloride; sodium hydrogensulfite; In ethanol; water;

Reference yield:

: 1402742-04-4
C₁₁H₁₂ClFO₄S

: 1402743-21-8
C₂₂H₂₆FNO₆S

Guidance literature:: Multi-step reaction with 5 steps

1.1: triethylamine / dichloromethane / 3 h / 0 - 25 °C

2.1: lithium diisopropyl amide / tetrahydrofuran / 0.5 h / -78 °C

3.1: sodium hexamethyldisilazane / tetrahydrofuran / 0.5 h / -78 - -30 °C

3.2: -78 - 25 °C

4.1: hydrogen / palladium hydrogenation catalyst / ethanol

5.1: diethoxyltriphenylphosphorane / toluene / 60 h / 45 °C

With diethoxyltriphenylphosphorane; hydrogen; sodium hexamethyldisilazane; triethylamine; lithium diisopropyl amide; palladium hydrogenation catalyst; In tetrahydrofuran; ethanol; dichloromethane; toluene;