N¹-Cyano-N²-<4-<(1,3-dihydro-5-methyl-2-oxo-3H-imidazol-4-yl)carbonyl>phenyl>-O-phenyl isourea

Base Information

• Chemical Name: N¹-Cyano-N²-<4-<(1,3-dihydro-5-methyl-2-oxo-3H-imidazol-4-yl)carbonyl>phenyl>-O-phenyl isourea
• CAS No.: 173375-92-3
• Molecular Formula: C₁₉H₁₅N₅O₃
• Molecular Weight: 361.36

Synonyms:N¹-Cyano-N²-<4-<(1,3-dihydro-5-methyl-2-oxo-3H-imidazol-4-yl)carbonyl>phenyl>-O-phenyl isourea

Chemical Property of N¹-Cyano-N²-<4-<(1,3-dihydro-5-methyl-2-oxo-3H-imidazol-4-yl)carbonyl>phenyl>-O-phenyl isourea

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Technology Process of N¹-Cyano-N²-<4-<(1,3-dihydro-5-methyl-2-oxo-3H-imidazol-4-yl)carbonyl>phenyl>-O-phenyl isourea

There total 5 articles about N¹-Cyano-N²-<4-<(1,3-dihydro-5-methyl-2-oxo-3H-imidazol-4-yl)carbonyl>phenyl>-O-phenyl isourea which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

N-cyanodiphenylcarbonimidate (79463-77-7) + 4-(4-Aminobenzoyl)-1,3-dihydro-5-methyl-3H-imidazol-2-one (173375-23-0) → N1-Cyano-N2-<4-<(1,3-dihydro-5-methyl-2-oxo-3H-imidazol-4-yl)carbonyl>phenyl>-O-phenyl isourea (173375-92-3)

Guidance literature:

With pyridine; for 5h; Ambient temperature;

DOI:10.1002/ardp.19953281005

Reference yield:

4–(1,3-dioxoisoindolin-2-yl)benzoyl chloride (5383-83-5) → N1-Cyano-N2-<4-<(1,3-dihydro-5-methyl-2-oxo-3H-imidazol-4-yl)carbonyl>phenyl>-O-phenyl isourea (173375-92-3)

Guidance literature:

Multi-step reaction with 3 steps

1: 88 percent / AlCl₃ / nitrobenzene / 6 h / 60 °C

2: 85 percent / 1 M aq. Na₂CO₃, hydrazine hydrate / 10 h / Ambient temperature

3: 95 percent / pyridine / 5 h / Ambient temperature

With pyridine; aluminium trichloride; sodium carbonate; hydrazine hydrate; In nitrobenzene;

DOI:10.1002/ardp.19953281005

Reference yield:

N-<4-<(1,3-Dihydro-5-methyl-2-oxo-3H-imidazol-4-yl)carbonyl>phenyl>-4-phthalimidobutanamide (173375-29-6) → N1-Cyano-N2-<4-<(1,3-dihydro-5-methyl-2-oxo-3H-imidazol-4-yl)carbonyl>phenyl>-O-phenyl isourea (173375-92-3)

Guidance literature:

Multi-step reaction with 4 steps

1: 40 percent / 1 M aq. Na₂CO₃, hydrazine hydrate / 24 h / Ambient temperature

2: 1.) MeCN, r.t., 2.) reflux, 20 h

3: 1 M aq. HCl

4: 95 percent / pyridine / 5 h / Ambient temperature

With pyridine; hydrogenchloride; sodium carbonate; hydrazine hydrate;

DOI:10.1002/ardp.19953281005

upstream raw materials:

N-cyanodiphenylcarbonimidate

4-(4-Aminobenzoyl)-1,3-dihydro-5-methyl-3H-imidazol-2-one

4–(1,3-dioxoisoindolin-2-yl)benzoyl chloride

N-<4-<(1,3-Dihydro-5-methyl-2-oxo-3H-imidazol-4-yl)carbonyl>phenyl>-4-phthalimidobutanamide

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