Technology Process of Acetic acid (1S,2R,3S,4R,5R,6R)-3,4-dihydroxy-2,5,6-tris-phosphonooxy-cyclohexyl ester
There total 3 articles about Acetic acid (1S,2R,3S,4R,5R,6R)-3,4-dihydroxy-2,5,6-tris-phosphonooxy-cyclohexyl ester which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
hydrogen;
palladium on activated charcoal;
In
acetic acid;
for 3h;
Ambient temperature;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: pyridine, 3 Angstroem and 4 Angstroem molecular sieves / toluene / 96 h / Ambient temperature; porcine pancreatic lipase
2: 1H-tetrazole / acetonitrile / 2 h / Ambient temperature
3: 30percent CH3CO3H / acetonitrile
4: 95 percent / H2 / 10percent Pd/C / acetic acid / 3 h / Ambient temperature
With
pyridine; 1H-tetrazole; peracetic acid; molecular sieve; hydrogen;
palladium on activated charcoal;
In
acetic acid; toluene; acetonitrile;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 1H-tetrazole / acetonitrile / 2 h / Ambient temperature
2: 30percent CH3CO3H / acetonitrile
3: 95 percent / H2 / 10percent Pd/C / acetic acid / 3 h / Ambient temperature
With
1H-tetrazole; peracetic acid; hydrogen;
palladium on activated charcoal;
In
acetic acid; acetonitrile;