Sodium; 4-(3-biphenyl-4-yl-2-mercaptomethyl-propionylamino)-benzenesulfonate

Base Information

Chemical Name:Sodium; 4-(3-biphenyl-4-yl-2-mercaptomethyl-propionylamino)-benzenesulfonate
CAS No.:126772-47-2
Molecular Formula:C₂₂H₂₀NO₄S₂*Na
Molecular Weight:449.527
Hs Code.:

Synonyms:Sodium; 4-(3-biphenyl-4-yl-2-mercaptomethyl-propionylamino)-benzenesulfonate

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Chemical Property of Sodium; 4-(3-biphenyl-4-yl-2-mercaptomethyl-propionylamino)-benzenesulfonate

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Technology Process of Sodium; 4-(3-biphenyl-4-yl-2-mercaptomethyl-propionylamino)-benzenesulfonate

There total 4 articles about Sodium; 4-(3-biphenyl-4-yl-2-mercaptomethyl-propionylamino)-benzenesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

: 126772-46-1
Sodium; 4-(2-acetylsulfanylmethyl-3-biphenyl-4-yl-propionylamino)-benzenesulfonate

: 126772-47-2
Sodium; 4-(3-biphenyl-4-yl-2-mercaptomethyl-propionylamino)-benzenesulfonate

Guidance literature:: With sodium hydroxide; In water; for 0.5h; Ambient temperature;
DOI:10.1021/jm00081a024

Reference yield:

: 115369-84-1
α-methylene-(1,1'-biphenyl)-4-propanoic acid

: 126772-47-2
Sodium; 4-(3-biphenyl-4-yl-2-mercaptomethyl-propionylamino)-benzenesulfonate

Guidance literature:: Multi-step reaction with 4 steps

1: 1 h / 80 °C

2: SOCl₂ / CHCl₃; dimethylformamide / 0.5 h / Heating

3: aq. NaOH / tetrahydrofuran / 0.5 h / Ambient temperature

4: 53 percent / 1N aq. NaOH / H₂O / 0.5 h / Ambient temperature

With sodium hydroxide; thionyl chloride; In tetrahydrofuran; chloroform; water; N,N-dimethyl-formamide;
DOI:10.1021/jm00081a024

Reference yield:

: 115355-26-5
(RS)-2-(acetylthiomethyl)-3-(4-phenyl phenyl)propanoic acid

: 126772-47-2
Sodium; 4-(3-biphenyl-4-yl-2-mercaptomethyl-propionylamino)-benzenesulfonate

Guidance literature:: Multi-step reaction with 3 steps

1: SOCl₂ / CHCl₃; dimethylformamide / 0.5 h / Heating

2: aq. NaOH / tetrahydrofuran / 0.5 h / Ambient temperature

3: 53 percent / 1N aq. NaOH / H₂O / 0.5 h / Ambient temperature

With sodium hydroxide; thionyl chloride; In tetrahydrofuran; chloroform; water; N,N-dimethyl-formamide;
DOI:10.1021/jm00081a024