(-)-10-(Dicyclohexylsulfamoyl)-D-isobornyl 2-oxophenylacetate tosylhydrazone

Base Information

Chemical Name:(-)-10-(Dicyclohexylsulfamoyl)-D-isobornyl 2-oxophenylacetate tosylhydrazone
CAS No.:170157-71-8
Molecular Formula:C₃₇H₅₁N₃O₆S₂
Molecular Weight:697.96
Hs Code.:

Synonyms:(-)-10-(Dicyclohexylsulfamoyl)-D-isobornyl 2-oxophenylacetate tosylhydrazone

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Chemical Property of (-)-10-(Dicyclohexylsulfamoyl)-D-isobornyl 2-oxophenylacetate tosylhydrazone

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Technology Process of (-)-10-(Dicyclohexylsulfamoyl)-D-isobornyl 2-oxophenylacetate tosylhydrazone

There total 3 articles about (-)-10-(Dicyclohexylsulfamoyl)-D-isobornyl 2-oxophenylacetate tosylhydrazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 1576-35-8
toluene-4-sulfonic acid hydrazide

: 170157-69-4
(-)-10-(Dicyclohexylsulfamoyl)-D-isobornyl 2-oxophenylacetate

: 170157-71-8
(-)-10-(Dicyclohexylsulfamoyl)-D-isobornyl 2-oxophenylacetate tosylhydrazone

Guidance literature:: In toluene; Heating;
DOI:10.1021/jo00119a023

Reference yield:

: 25726-04-9
phenylglyoxylyl chloride

: 170157-71-8
(-)-10-(Dicyclohexylsulfamoyl)-D-isobornyl 2-oxophenylacetate tosylhydrazone

Guidance literature:: Multi-step reaction with 2 steps

1: 86 percent / pyridine, DMAP / CH₂Cl₂ / 15 h / Heating

2: 74 percent / toluene / Heating

With pyridine; dmap; In dichloromethane; toluene;
DOI:10.1021/jo00119a023

Reference yield:

: 96303-88-7
(-)-10-dicyclohexylsulfamoyl-D-isoborneol

: 170157-71-8
(-)-10-(Dicyclohexylsulfamoyl)-D-isobornyl 2-oxophenylacetate tosylhydrazone

Guidance literature:: Multi-step reaction with 2 steps

1: 86 percent / pyridine, DMAP / CH₂Cl₂ / 15 h / Heating

2: 74 percent / toluene / Heating

With pyridine; dmap; In dichloromethane; toluene;
DOI:10.1021/jo00119a023