allyl 3-O-[2-O-benzoyl-3,4,6-tri-O-benzyl-β-D-glucopyranosyl-(1->2)-3,4-di-O-benzoyl-β-L-arabinopyranosyl]-23-O-benzoylhederagenate

Base Information

Chemical Name:allyl 3-O-[2-O-benzoyl-3,4,6-tri-O-benzyl-β-D-glucopyranosyl-(1->2)-3,4-di-O-benzoyl-β-L-arabinopyranosyl]-23-O-benzoylhederagenate
CAS No.:852448-41-0
Molecular Formula:C₉₃H₁₀₄O₁₇
Molecular Weight:1493.84
Hs Code.:

Synonyms:allyl 3-O-[2-O-benzoyl-3,4,6-tri-O-benzyl-β-D-glucopyranosyl-(1->2)-3,4-di-O-benzoyl-β-L-arabinopyranosyl]-23-O-benzoylhederagenate

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Chemical Property of allyl 3-O-[2-O-benzoyl-3,4,6-tri-O-benzyl-β-D-glucopyranosyl-(1->2)-3,4-di-O-benzoyl-β-L-arabinopyranosyl]-23-O-benzoylhederagenate

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Technology Process of allyl 3-O-[2-O-benzoyl-3,4,6-tri-O-benzyl-β-D-glucopyranosyl-(1->2)-3,4-di-O-benzoyl-β-L-arabinopyranosyl]-23-O-benzoylhederagenate

There total 2 articles about allyl 3-O-[2-O-benzoyl-3,4,6-tri-O-benzyl-β-D-glucopyranosyl-(1->2)-3,4-di-O-benzoyl-β-L-arabinopyranosyl]-23-O-benzoylhederagenate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 852448-33-0
2-O-benzoyl-3,4,6-tri-O-benzyl-β-D-glucopyranosyl-(1->2)-3,4-di-O-benzoyl-β-L-arabinopyranosyl trichloroacetimidate

: allyl 23-O-benzoylhederagenate

: 852448-41-0
allyl 3-O-[2-O-benzoyl-3,4,6-tri-O-benzyl-β-D-glucopyranosyl-(1->2)-3,4-di-O-benzoyl-β-L-arabinopyranosyl]-23-O-benzoylhederagenate

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; 4 A molecular sieve; In dichloromethane; at 0 ℃; for 6h;
DOI:10.1016/j.tet.2005.03.003

Reference yield: 61.0%

: 852448-33-0
2-O-benzoyl-3,4,6-tri-O-benzyl-β-D-glucopyranosyl-(1->2)-3,4-di-O-benzoyl-β-L-arabinopyranosyl trichloroacetimidate

: allyl 23-O-benzoylhederagenate

: allyl 3-O-[2-O-benzoyl-3,4,6-tri-O-benzyl-β-D-glucopyranosyl-(1->2)-3,4-di-O-benzoyl-α-L-arabinopyranosyl]-23-O-benzoylhederagenate

: 852448-41-0
allyl 3-O-[2-O-benzoyl-3,4,6-tri-O-benzyl-β-D-glucopyranosyl-(1->2)-3,4-di-O-benzoyl-β-L-arabinopyranosyl]-23-O-benzoylhederagenate

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; 4 A molecular sieve; In acetonitrile; at -35 ℃; for 6h;
DOI:10.1016/j.tet.2005.03.003

Reference yield: 88.0%

: 852448-41-0
allyl 3-O-[2-O-benzoyl-3,4,6-tri-O-benzyl-β-D-glucopyranosyl-(1->2)-3,4-di-O-benzoyl-β-L-arabinopyranosyl]-23-O-benzoylhederagenate

: 20853-58-1
3-O-[β-D-glucopyranosyl-(1->2)-β-L-arabinopyranosyl]-hederagenin

Guidance literature:: allyl 3-O-[2-O-benzoyl-3,4,6-tri-O-benzyl-β-D-glucopyranosyl-(1->2)-3,4-di-O-benzoyl-β-L-arabinopyranosyl]-23-O-benzoylhederagenate; With potassium hydroxide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In methanol; at 60 ℃; for 6h;

With hydrogen; palladium on activated charcoal; In ethanol; at 20 ℃; for 48h;
DOI:10.1016/j.tet.2005.03.003