2-pentafluorobenzoyl-7-(5-n-nonyl-thiophene-2-yl)-benzo[2,1-b:3,4-b']dithiazole-4,5-bis(ethyleneoxolane)

Base Information

Chemical Name:2-pentafluorobenzoyl-7-(5-n-nonyl-thiophene-2-yl)-benzo[2,1-b:3,4-b']dithiazole-4,5-bis(ethyleneoxolane)
CAS No.:1422378-84-4
Molecular Formula:C₃₄H₃₁F₅O₅S₃
Molecular Weight:710.807
Hs Code.:

Synonyms:2-pentafluorobenzoyl-7-(5-n-nonyl-thiophene-2-yl)-benzo[2,1-b:3,4-b']dithiazole-4,5-bis(ethyleneoxolane)

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Chemical Property of 2-pentafluorobenzoyl-7-(5-n-nonyl-thiophene-2-yl)-benzo[2,1-b:3,4-b']dithiazole-4,5-bis(ethyleneoxolane)

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Technology Process of 2-pentafluorobenzoyl-7-(5-n-nonyl-thiophene-2-yl)-benzo[2,1-b:3,4-b']dithiazole-4,5-bis(ethyleneoxolane)

There total 6 articles about 2-pentafluorobenzoyl-7-(5-n-nonyl-thiophene-2-yl)-benzo[2,1-b:3,4-b']dithiazole-4,5-bis(ethyleneoxolane) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.8%

: 1422378-77-5
2-bromo-7-pentafluorobenzoyl-bis-benzo[2,1-b:3,4-b]dithiophene-4,5-bis(ethyleneoxolane)

: 2-(5-nonylthiophen-2-yl)-5-tributylstannanylpyridine

: 1422378-84-4
2-pentafluorobenzoyl-7-(5-n-nonyl-thiophene-2-yl)-benzo[2,1-b:3,4-b']dithiazole-4,5-bis(ethyleneoxolane)

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; In N,N-dimethyl-formamide; Inert atmosphere; Reflux;

Reference yield:

: 1258459-49-2
2,5-dibromo-benzo-[2,1-b:3,4-b′]dithiophene-7,8-quinone

: 1422378-84-4
2-pentafluorobenzoyl-7-(5-n-nonyl-thiophene-2-yl)-benzo[2,1-b:3,4-b']dithiazole-4,5-bis(ethyleneoxolane)

Guidance literature:: Multi-step reaction with 3 steps

1.1: toluene-4-sulfonic acid / toluene / Reflux

2.1: n-butyllithium / tetrahydrofuran; hexane / 0.25 h / Cooling with acetone-dry ice; Inert atmosphere

2.2: 20 °C

3.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾ / N,N-dimethyl-formamide / Inert atmosphere; Reflux

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; n-butyllithium; toluene-4-sulfonic acid; In tetrahydrofuran; hexane; N,N-dimethyl-formamide; toluene;

Reference yield:

: 1187970-52-0
2,7-bis-trimethylsilyl-benzo [1,2-b:6,5-b’] dithiophene-4,5-dione

: 1422378-84-4
2-pentafluorobenzoyl-7-(5-n-nonyl-thiophene-2-yl)-benzo[2,1-b:3,4-b']dithiazole-4,5-bis(ethyleneoxolane)

Guidance literature:: Multi-step reaction with 4 steps

1.1: bromine / dichloromethane / Cooling with liquid nitrogen

2.1: toluene-4-sulfonic acid / toluene / Reflux

3.1: n-butyllithium / tetrahydrofuran; hexane / 0.25 h / Cooling with acetone-dry ice; Inert atmosphere

3.2: 20 °C

4.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾ / N,N-dimethyl-formamide / Inert atmosphere; Reflux

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; n-butyllithium; bromine; toluene-4-sulfonic acid; In tetrahydrofuran; hexane; dichloromethane; N,N-dimethyl-formamide; toluene;