2-phenyl-4-[3-S-(tert-butoxycarbonyl)mercaptobenzoyl]amino-3'-carboxybiphenyl

Base Information

Chemical Name:2-phenyl-4-[3-S-(tert-butoxycarbonyl)mercaptobenzoyl]amino-3'-carboxybiphenyl
CAS No.:323191-91-9
Molecular Formula:C₃₁H₂₇NO₅S
Molecular Weight:525.625
Hs Code.:

Synonyms:2-phenyl-4-[3-S-(tert-butoxycarbonyl)mercaptobenzoyl]amino-3'-carboxybiphenyl

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Chemical Property of 2-phenyl-4-[3-S-(tert-butoxycarbonyl)mercaptobenzoyl]amino-3'-carboxybiphenyl

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Technology Process of 2-phenyl-4-[3-S-(tert-butoxycarbonyl)mercaptobenzoyl]amino-3'-carboxybiphenyl

There total 9 articles about 2-phenyl-4-[3-S-(tert-butoxycarbonyl)mercaptobenzoyl]amino-3'-carboxybiphenyl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 29608-75-1
2-amino-5-nitro-biphenyl

: 323191-91-9
2-phenyl-4-[3-S-(tert-butoxycarbonyl)mercaptobenzoyl]amino-3'-carboxybiphenyl

Guidance literature:: Multi-step reaction with 5 steps

1.1: H₂SO₄ conc.; NaNO₂ / acetic acid / 1 h / 10 °C

1.2: 77 percent / KI / aq. HCl / 20 - 70 °C

2.1: 95 percent / Pd(OAc)2 / acetone; H₂O / Heating

4.1: 62 percent / SnCl₂ / ethyl acetate; ethanol / 2 h / Heating

5.1: 24 mg / tetrahydrofuran / -15 - 20 °C

With palladium diacetate; sulfuric acid; tin(ll) chloride; sodium nitrite; In tetrahydrofuran; ethanol; water; acetic acid; ethyl acetate; acetone; 1.1: Diazotization / 1.2: Substitution / 2.1: Substitution / 4.1: Reduction / 5.1: Condensation;
DOI:10.1016/S0040-4020(00)00890-5

Reference yield:

: 13296-94-1
2-bromo-4-nitroaniline

: 323191-91-9
2-phenyl-4-[3-S-(tert-butoxycarbonyl)mercaptobenzoyl]amino-3'-carboxybiphenyl

Guidance literature:: Multi-step reaction with 6 steps

1.1: 75 percent / Pd(OAc)2 / acetone; H₂O / Heating

2.1: H₂SO₄ conc.; NaNO₂ / acetic acid / 1 h / 10 °C

2.2: 77 percent / KI / aq. HCl / 20 - 70 °C

3.1: 95 percent / Pd(OAc)2 / acetone; H₂O / Heating

5.1: 62 percent / SnCl₂ / ethyl acetate; ethanol / 2 h / Heating

6.1: 24 mg / tetrahydrofuran / -15 - 20 °C

With palladium diacetate; sulfuric acid; tin(ll) chloride; sodium nitrite; In tetrahydrofuran; ethanol; water; acetic acid; ethyl acetate; acetone; 1.1: Substitution / 2.1: Diazotization / 2.2: Substitution / 3.1: Substitution / 5.1: Reduction / 6.1: Condensation;
DOI:10.1016/S0040-4020(00)00890-5

Reference yield:

: 323191-82-8
1-iodo-2-phenyl-4-nitrobenzene

: 323191-91-9
2-phenyl-4-[3-S-(tert-butoxycarbonyl)mercaptobenzoyl]amino-3'-carboxybiphenyl

Guidance literature:: Multi-step reaction with 4 steps

1: 95 percent / Pd(OAc)2 / acetone; H₂O / Heating

3: 62 percent / SnCl₂ / ethyl acetate; ethanol / 2 h / Heating

4: 24 mg / tetrahydrofuran / -15 - 20 °C

With palladium diacetate; tin(ll) chloride; In tetrahydrofuran; ethanol; water; ethyl acetate; acetone; 1: Substitution / 3: Reduction / 4: Condensation;
DOI:10.1016/S0040-4020(00)00890-5