19-benzyl-16,19-dihydro-2,13-diaza<4>paracyclo<4>(3,5)pyridinophane-1,14-dione

Base Information

Chemical Name:19-benzyl-16,19-dihydro-2,13-diaza<4>paracyclo<4>(3,5)pyridinophane-1,14-dione
CAS No.:75340-05-5
Molecular Formula:C₂₄H₂₅N₃O₂
Molecular Weight:387.481
Hs Code.:

Synonyms:19-benzyl-16,19-dihydro-2,13-diaza<4>paracyclo<4>(3,5)pyridinophane-1,14-dione

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Chemical Property of 19-benzyl-16,19-dihydro-2,13-diaza<4>paracyclo<4>(3,5)pyridinophane-1,14-dione

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Technology Process of 19-benzyl-16,19-dihydro-2,13-diaza<4>paracyclo<4>(3,5)pyridinophane-1,14-dione

There total 4 articles about 19-benzyl-16,19-dihydro-2,13-diaza<4>paracyclo<4>(3,5)pyridinophane-1,14-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

: 8-Benzyl-5,11-dioxo-4,12-diaza-8-azonia-tricyclo[13.2.2.1^6,10]icosa-1⁽¹⁸⁾,6,8,10⁽²⁰⁾,15⁽¹⁹⁾,16-hexaene; bromide

: 75340-05-5
19-benzyl-16,19-dihydro-2,13-diaza<4>paracyclo<4>(3,5)pyridinophane-1,14-dione

Guidance literature:: With 1-Benzyl-1,4-dihydronicotinamide; In methanol; at 50 ℃; for 3h; dark;
DOI:10.1021/ja00325a020

Reference yield:

: 15074-61-0
pyridine-3,5-dicarbonyl dichloride

: 75340-05-5
19-benzyl-16,19-dihydro-2,13-diaza<4>paracyclo<4>(3,5)pyridinophane-1,14-dione

Guidance literature:: Multi-step reaction with 3 steps

1: 3 percent / triethylamine / toluene / 50 h / Ambient temperature

2: 67 percent / 1 h / 80 °C

3: β-NADH / H2O / 20 °C / pH=7

With 1,4-dihydronicotinamide adenine dinucleotide; triethylamine; In water; toluene;
DOI:10.1021/ja00325a020

Reference yield:

: 499-81-0
3,5-Pyridinedicarboxylic acid

: 75340-05-5
19-benzyl-16,19-dihydro-2,13-diaza<4>paracyclo<4>(3,5)pyridinophane-1,14-dione

Guidance literature:: Multi-step reaction with 4 steps

1: 85 percent / tionyl chloride / Heating

2: 3 percent / triethylamine / toluene / 50 h / Ambient temperature

3: 67 percent / 1 h / 80 °C

4: β-NADH / H2O / 20 °C / pH=7

With thionyl chloride; 1,4-dihydronicotinamide adenine dinucleotide; triethylamine; In water; toluene;
DOI:10.1021/ja00325a020