C₄₅H₅₄O₈

Base Information

Chemical Name:C₄₅H₅₄O₈
CAS No.:1611466-21-7
Molecular Formula:C₄₅H₅₄O₈
Molecular Weight:722.919
Hs Code.:

C<sub>45</sub>H<sub>54</sub>O<sub>8</sub>

Synonyms:C₄₅H₅₄O₈

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Chemical Property of C₄₅H₅₄O₈

Chemical Property:

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Technology Process of C₄₅H₅₄O₈

There total 13 articles about C₄₅H₅₄O₈ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: C₄₅H₅₆O₈

: 1611466-21-7
C₄₅H₅₄O₈

Guidance literature:: With sodium hydrogencarbonate; Dess-Martin periodane; In dichloromethane; at 20 ℃; for 1h; Inert atmosphere;
DOI:10.1002/chem.201304776

Reference yield:

: 29048-54-2
1-(2,4-dihydroxyphenyl)-2-methyl-1-propanone

: 1611466-21-7
C₄₅H₅₄O₈

Guidance literature:: Multi-step reaction with 8 steps

1.1: sodium cyanoborohydride; methyl orange; hydrogenchloride / methanol; water / 24 h

2.1: potassium carbonate / N,N-dimethyl-formamide

3.1: N,N,N,N,-tetramethylethylenediamine; n-butyllithium / diethyl ether; hexane / 0.5 h / 0 °C / Inert atmosphere

3.2: 2 h / Inert atmosphere

4.1: N-Bromosuccinimide / chloroform / 23 h / Inert atmosphere; Darkness

5.1: tert.-butyl lithium / tetrahydrofuran; pentane / 0.25 h / -78 °C / Inert atmosphere

5.2: 0.75 h / -78 °C / Inert atmosphere

6.1: diisobutylaluminium hydride / n-heptane; methanol; toluene / 1.75 h / -78 - 0 °C / Inert atmosphere

7.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 2 h / 0 - 20 °C

8.1: sodium hydrogencarbonate; Dess-Martin periodane / dichloromethane / 1 h / 20 °C / Inert atmosphere

With hydrogenchloride; N-Bromosuccinimide; n-butyllithium; N,N,N,N,-tetramethylethylenediamine; tetrabutyl ammonium fluoride; methyl orange; tert.-butyl lithium; diisobutylaluminium hydride; sodium cyanoborohydride; sodium hydrogencarbonate; potassium carbonate; Dess-Martin periodane; In tetrahydrofuran; methanol; diethyl ether; hexane; n-heptane; dichloromethane; chloroform; water; N,N-dimethyl-formamide; toluene; pentane;
DOI:10.1002/chem.201304776

Reference yield:

: 1611465-60-1
C₂₉H₅₈O₆Si₂

: 1611466-21-7
C₄₅H₅₄O₈

Guidance literature:: Multi-step reaction with 4 steps

1.1: tert.-butyl lithium / tetrahydrofuran; pentane / 0.25 h / -78 °C / Inert atmosphere

1.2: 0.75 h / -78 °C / Inert atmosphere

2.1: diisobutylaluminium hydride / n-heptane; methanol; toluene / 1.75 h / -78 - 0 °C / Inert atmosphere

3.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 2 h / 0 - 20 °C

4.1: sodium hydrogencarbonate; Dess-Martin periodane / dichloromethane / 1 h / 20 °C / Inert atmosphere

With tetrabutyl ammonium fluoride; tert.-butyl lithium; diisobutylaluminium hydride; sodium hydrogencarbonate; Dess-Martin periodane; In tetrahydrofuran; methanol; n-heptane; dichloromethane; toluene; pentane;
DOI:10.1002/chem.201304776