C₄₁H₅₀N₂O₁₀

Base Information

Chemical Name:C₄₁H₅₀N₂O₁₀
CAS No.:943000-44-0
Molecular Formula:C₄₁H₅₀N₂O₁₀
Molecular Weight:730.855
Hs Code.:

C<sub>41</sub>H<sub>50</sub>N<sub>2</sub>O<sub>10</sub>

Synonyms:C₄₁H₅₀N₂O₁₀

Suppliers and Price of C₄₁H₅₀N₂O₁₀

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₄₁H₅₀N₂O₁₀

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₄₁H₅₀N₂O₁₀

There total 15 articles about C₄₁H₅₀N₂O₁₀ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 78179-60-9
3β-acetoxy-12α-hydroxy-5α-spirostan-14-ene

: 943000-44-0
C₄₁H₅₀N₂O₁₀

Guidance literature:: Multi-step reaction with 11 steps

1.1: Jones reagent / acetone / 0 - 23 °C

2.1: sodium borohydride / CH₂Cl₂; methanol / -90 - 23 °C

3.1: 10.5 g / 4-N,N-dimethylaminopyridine / CH₂Cl₂; pyridine / 4.5 h / 23 °C

4.1: 93 percent / NaCNBH₃; acetic acid / 2.5 h

5.1: tributylphosphine; 2-nitrophenyl selenocyanate; pyridine / 40 h / 23 °C

5.2: 67 percent / aq. H₂O₂ / CH₂Cl₂ / 0 - 11 °C

6.1: mercury(II) acetate / tetrahydrofuran; H₂O / 16 h / 23 °C

6.2: 88 percent / NaBH₄ / tetrahydrofuran; H₂O / 3 h

7.1: 28 percent / iodine; iodobenzene diacetate / hexane; CH₂Cl₂ / 2 h

8.1: 100 percent / potassium carbonate; methanol / tetrahydrofuran / 24 h / 40 °C

9.1: MgSO₄ / benzene / 72 h / 23 °C

10.1: 90 percent / CH₂Cl₂; pyridine / 24 h / 45 °C

11.1: magnesium sulfate; NaCNBH₃; acetic acid / toluene / 16 h / 23 °C

With pyridine; methanol; sodium tetrahydroborate; ortho-nitrophenyl selenocyanate; jones reagent; tributylphosphine; [bis(acetoxy)iodo]benzene; mercury(II) diacetate; iodine; sodium cyanoborohydride; magnesium sulfate; potassium carbonate; acetic acid; dmap; In tetrahydrofuran; pyridine; methanol; hexane; dichloromethane; water; acetone; toluene; benzene; 1.1: Jones oxidation / 5.1: Grieco reaction / 7.1: Suarez iodine(III) oxidation;
DOI:10.1021/ja0705487

Reference yield:

: 78179-61-0
3β-acetoxy-12-keto-5α-spirostan-14-ene

: 943000-44-0
C₄₁H₅₀N₂O₁₀

Guidance literature:: Multi-step reaction with 10 steps

1.1: sodium borohydride / CH₂Cl₂; methanol / -90 - 23 °C

2.1: 10.5 g / 4-N,N-dimethylaminopyridine / CH₂Cl₂; pyridine / 4.5 h / 23 °C

3.1: 93 percent / NaCNBH₃; acetic acid / 2.5 h

4.1: tributylphosphine; 2-nitrophenyl selenocyanate; pyridine / 40 h / 23 °C

4.2: 67 percent / aq. H₂O₂ / CH₂Cl₂ / 0 - 11 °C

5.1: mercury(II) acetate / tetrahydrofuran; H₂O / 16 h / 23 °C

5.2: 88 percent / NaBH₄ / tetrahydrofuran; H₂O / 3 h

6.1: 28 percent / iodine; iodobenzene diacetate / hexane; CH₂Cl₂ / 2 h

7.1: 100 percent / potassium carbonate; methanol / tetrahydrofuran / 24 h / 40 °C

8.1: MgSO₄ / benzene / 72 h / 23 °C

9.1: 90 percent / CH₂Cl₂; pyridine / 24 h / 45 °C

10.1: magnesium sulfate; NaCNBH₃; acetic acid / toluene / 16 h / 23 °C

With pyridine; methanol; sodium tetrahydroborate; ortho-nitrophenyl selenocyanate; tributylphosphine; [bis(acetoxy)iodo]benzene; mercury(II) diacetate; iodine; sodium cyanoborohydride; magnesium sulfate; potassium carbonate; acetic acid; dmap; In tetrahydrofuran; pyridine; methanol; hexane; dichloromethane; water; toluene; benzene; 4.1: Grieco reaction / 6.1: Suarez iodine(III) oxidation;
DOI:10.1021/ja0705487

Reference yield:

: 6917-04-0
(25R)-3β-Acetoxy-12,13-seco-5α-spirost-13-en-12-on

: 943000-44-0
C₄₁H₅₀N₂O₁₀

Guidance literature:: Multi-step reaction with 12 steps

1.1: 1.58 g / boron trifluoride diethyl etherate / toluene / 1 h / 0 °C

2.1: Jones reagent / acetone / 0 - 23 °C

3.1: sodium borohydride / CH₂Cl₂; methanol / -90 - 23 °C

4.1: 10.5 g / 4-N,N-dimethylaminopyridine / CH₂Cl₂; pyridine / 4.5 h / 23 °C

5.1: 93 percent / NaCNBH₃; acetic acid / 2.5 h

6.1: tributylphosphine; 2-nitrophenyl selenocyanate; pyridine / 40 h / 23 °C

6.2: 67 percent / aq. H₂O₂ / CH₂Cl₂ / 0 - 11 °C

7.1: mercury(II) acetate / tetrahydrofuran; H₂O / 16 h / 23 °C

7.2: 88 percent / NaBH₄ / tetrahydrofuran; H₂O / 3 h

8.1: 28 percent / iodine; iodobenzene diacetate / hexane; CH₂Cl₂ / 2 h

9.1: 100 percent / potassium carbonate; methanol / tetrahydrofuran / 24 h / 40 °C

10.1: MgSO₄ / benzene / 72 h / 23 °C

11.1: 90 percent / CH₂Cl₂; pyridine / 24 h / 45 °C

12.1: magnesium sulfate; NaCNBH₃; acetic acid / toluene / 16 h / 23 °C

With pyridine; methanol; sodium tetrahydroborate; ortho-nitrophenyl selenocyanate; jones reagent; tributylphosphine; [bis(acetoxy)iodo]benzene; mercury(II) diacetate; iodine; sodium cyanoborohydride; magnesium sulfate; potassium carbonate; acetic acid; dmap; boron trifluoride diethyl etherate; In tetrahydrofuran; pyridine; methanol; hexane; dichloromethane; water; acetone; toluene; benzene; 2.1: Jones oxidation / 6.1: Grieco reaction / 8.1: Suarez iodine(III) oxidation;
DOI:10.1021/ja0705487