tert-butyl 2-((tert-butoxycarbonyl)(1-phenylethyl)amino)-4-(5-(1-(2-(4-pentylbenzamido)ethyl)-1H-1,2,3-triazol-4-yl)pentyl)-1H-imidazole-1-carboxylate

Base Information

Chemical Name:tert-butyl 2-((tert-butoxycarbonyl)(1-phenylethyl)amino)-4-(5-(1-(2-(4-pentylbenzamido)ethyl)-1H-1,2,3-triazol-4-yl)pentyl)-1H-imidazole-1-carboxylate
CAS No.:1415901-37-9
Molecular Formula:C₄₂H₅₉N₇O₅
Molecular Weight:741.974
Hs Code.:

tert-butyl 2-((tert-butoxycarbonyl)(1-phenylethyl)amino)-4-(5-(1-(2-(4-pentylbenzamido)ethyl)-1H-1,2,3-triazol-4-yl)pentyl)-1H-imidazole-1-carboxylate

Synonyms:tert-butyl 2-((tert-butoxycarbonyl)(1-phenylethyl)amino)-4-(5-(1-(2-(4-pentylbenzamido)ethyl)-1H-1,2,3-triazol-4-yl)pentyl)-1H-imidazole-1-carboxylate

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Chemical Property of tert-butyl 2-((tert-butoxycarbonyl)(1-phenylethyl)amino)-4-(5-(1-(2-(4-pentylbenzamido)ethyl)-1H-1,2,3-triazol-4-yl)pentyl)-1H-imidazole-1-carboxylate

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Technology Process of tert-butyl 2-((tert-butoxycarbonyl)(1-phenylethyl)amino)-4-(5-(1-(2-(4-pentylbenzamido)ethyl)-1H-1,2,3-triazol-4-yl)pentyl)-1H-imidazole-1-carboxylate

There total 8 articles about tert-butyl 2-((tert-butoxycarbonyl)(1-phenylethyl)amino)-4-(5-(1-(2-(4-pentylbenzamido)ethyl)-1H-1,2,3-triazol-4-yl)pentyl)-1H-imidazole-1-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 1192358-22-7
N-(2-azidoethyl)-4-pentylbenzamide

: 1415901-05-1
C₂₈H₃₉N₃O₄

: 1415901-37-9
tert-butyl 2-((tert-butoxycarbonyl)(1-phenylethyl)amino)-4-(5-(1-(2-(4-pentylbenzamido)ethyl)-1H-1,2,3-triazol-4-yl)pentyl)-1H-imidazole-1-carboxylate

Guidance literature:: With copper(II) sulfate; sodium L-ascorbate; In dichloromethane; water; tert-butyl alcohol;
DOI:10.1039/c2ob26469b

Reference yield:

: 1415900-86-5
tert-butyl 2-((tert-butoxycarbonyl)amino)-4-(hept-6-yn-1-yl)-1H-imidazole-1-carboxylate

: 1415901-37-9
tert-butyl 2-((tert-butoxycarbonyl)(1-phenylethyl)amino)-4-(5-(1-(2-(4-pentylbenzamido)ethyl)-1H-1,2,3-triazol-4-yl)pentyl)-1H-imidazole-1-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydride / mineral oil; N,N-dimethyl-formamide / 0 °C

1.2: 4 h / 70 °C

2.1: copper(II) sulfate; sodium L-ascorbate / dichloromethane; water; tert-butyl alcohol

With sodium hydride; copper(II) sulfate; sodium L-ascorbate; In dichloromethane; water; N,N-dimethyl-formamide; mineral oil; tert-butyl alcohol; 2.1: |Huisgen Cycloaddition;
DOI:10.1039/c2ob26469b

Reference yield:

: 20739-58-6
2-octyn-1-ol

: 1415901-37-9
tert-butyl 2-((tert-butoxycarbonyl)(1-phenylethyl)amino)-4-(5-(1-(2-(4-pentylbenzamido)ethyl)-1H-1,2,3-triazol-4-yl)pentyl)-1H-imidazole-1-carboxylate

Guidance literature:: Multi-step reaction with 8 steps

1.1: ethylenediamine; sodium hydride

2.1: Jones reagent

3.1: oxalyl dichloride

4.1: diethyl ether; dichloromethane / 0 °C

5.1: bromine / water

6.1: sodium hydride / mineral oil; tetrahydrofuran / 0.5 h / 0 °C

6.2: 4 h / 0 - 25 °C

6.3: 1 h / -78 °C

7.1: sodium hydride / mineral oil; N,N-dimethyl-formamide / 0 °C

7.2: 4 h / 70 °C

8.1: copper(II) sulfate; sodium L-ascorbate / dichloromethane; water; tert-butyl alcohol

With Jones reagent; oxalyl dichloride; bromine; sodium hydride; copper(II) sulfate; sodium L-ascorbate; ethylenediamine; In tetrahydrofuran; diethyl ether; dichloromethane; water; N,N-dimethyl-formamide; mineral oil; tert-butyl alcohol; 8.1: |Huisgen Cycloaddition;
DOI:10.1039/c2ob26469b