C₆₉H₉₆O₉Si₃

Base Information

Chemical Name:C₆₉H₉₆O₉Si₃
CAS No.:1261152-32-2
Molecular Formula:C₆₉H₉₆O₉Si₃
Molecular Weight:1153.77
Hs Code.:

C<sub>69</sub>H<sub>96</sub>O<sub>9</sub>Si<sub>3</sub>

Synonyms:C₆₉H₉₆O₉Si₃

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Chemical Property of C₆₉H₉₆O₉Si₃

Chemical Property:

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Technology Process of C₆₉H₉₆O₉Si₃

There total 27 articles about C₆₉H₉₆O₉Si₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 557-91-5
1,1-Dibromoethane

: 1261152-50-4
C₇₁H₁₀₀O₁₀Si₃

: 1261152-32-2
C₆₉H₉₆O₉Si₃

Guidance literature:: With N,N,N,N,-tetramethylethylenediamine; titanium tetrachloride; In tetrahydrofuran; dichloromethane; at 0 - 25 ℃; Inert atmosphere;

With lead(II) chloride; zinc; In tetrahydrofuran; dichloromethane; at 25 ℃; for 0.666667h; Inert atmosphere;

1,1-Dibromoethane; C₇₁H₁₀₀O₁₀Si₃; Further stages;
DOI:10.1021/ja109533y

Reference yield:

: 557-91-5
1,1-Dibromoethane

: 1261152-50-4
C₇₁H₁₀₀O₁₀Si₃

: 1261152-32-2
C₆₉H₉₆O₉Si₃

: 1261152-31-1
C₇₃H₁₀₄O₉Si₃

Guidance literature:: With N,N,N,N,-tetramethylethylenediamine; titanium tetrachloride; In tetrahydrofuran; dichloromethane; at 0 - 25 ℃; Inert atmosphere;

With lead(II) chloride; zinc; In tetrahydrofuran; dichloromethane; at 25 ℃; for 0.666667h; Inert atmosphere;

1,1-Dibromoethane; C₇₁H₁₀₀O₁₀Si₃; Further stages;
DOI:10.1021/ja109533y

Reference yield:

: C₃₆H₅₆O₆Si₂

: 1261152-32-2
C₆₉H₉₆O₉Si₃

Guidance literature:: Multi-step reaction with 16 steps

1.1: 2,6-dimethylpyridine / dichloromethane / 14 h / 0 °C / Inert atmosphere

2.1: diisobutylaluminium hydride / dichloromethane / 1 h / -78 °C / Inert atmosphere

2.2: 16 h / 25 °C / Inert atmosphere

3.1: titanium(IV) isopropylate; diethyl (2S,3S)-tartrate / dichloromethane / 1 h / -25 °C / Inert atmosphere; Molecular sieve

3.2: 17 h / -20 °C / Inert atmosphere; Molecular sieve

4.1: sulfur trioxide pyridine complex; dimethyl sulfoxide; triethylamine / dichloromethane / 0 - 25 °C / Inert atmosphere

5.1: dichloromethane / 14 h / 20 °C / Inert atmosphere

6.1: tetrabutyl ammonium fluoride / dichloromethane / 0.33 h / 0 °C / Inert atmosphere

7.1: pyridinium p-toluenesulfonate / dichloromethane / 25 - 40 °C / Inert atmosphere

8.1: lanthanum(lll) triflate / toluene / 6 h / 25 °C / Inert atmosphere

9.1: sodium tetrahydroborate; nickel (II) chloride hexahydrate / ethanol / 0 °C / Inert atmosphere

10.1: lithium aluminium tetrahydride / tetrahydrofuran; diethyl ether / 0.5 h / 25 °C / Inert atmosphere

11.1: sulfur trioxide pyridine complex; dimethyl sulfoxide; triethylamine / dichloromethane / 0 - 25 °C / Inert atmosphere

12.1: sodium hexamethyldisilazane / tetrahydrofuran; toluene / 0.17 h / 0 °C / Inert atmosphere

12.2: 0.33 h / 0 °C / Inert atmosphere

13.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane / 3 h / 0 °C / Inert atmosphere

14.1: dmap; 2-methyl-6-nitrobenzoic anhydride; triethylamine / toluene / 0.33 h / 25 °C / Inert atmosphere; Molecular sieve

14.2: 13 h / 25 °C / Inert atmosphere; Molecular sieve

15.1: p-toluenesulfonic acid monohydrate / methanol; dichloromethane / 0.67 h / 0 °C / Inert atmosphere

16.1: N,N,N,N,-tetramethylethylenediamine; titanium tetrachloride / tetrahydrofuran; dichloromethane / 0 - 25 °C / Inert atmosphere

16.2: 0.67 h / 25 °C / Inert atmosphere

With 2,6-dimethylpyridine; titanium(IV) isopropylate; dmap; sodium tetrahydroborate; lithium aluminium tetrahydride; nickel (II) chloride hexahydrate; diethyl (2S,3S)-tartrate; N,N,N,N,-tetramethylethylenediamine; 2-methyl-6-nitrobenzoic anhydride; p-toluenesulfonic acid monohydrate; tetrabutyl ammonium fluoride; sodium hexamethyldisilazane; sulfur trioxide pyridine complex; pyridinium p-toluenesulfonate; titanium tetrachloride; diisobutylaluminium hydride; dimethyl sulfoxide; triethylamine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; lanthanum(lll) triflate; In tetrahydrofuran; methanol; diethyl ether; ethanol; dichloromethane; toluene; 3.1: Sharpless epoxidation / 3.2: Sharpless epoxidation / 4.1: Parikh-Doering oxidation / 5.1: Wittig reaction / 11.1: Parikh-Doering oxidation / 12.1: Wittig reaction / 12.2: Wittig reaction;
DOI:10.1021/ja109533y