4'-(4-iodo-benzoyloxy)-biphenyl-4-carboxylic acid nonyl ester

Base Information

• Chemical Name: 4'-(4-iodo-benzoyloxy)-biphenyl-4-carboxylic acid nonyl ester
• CAS No.: 727668-65-7
• Molecular Formula: C₂₉H₃₁IO₄
• Molecular Weight: 570.467
• Mol file: 727668-65-7.mol

Synonyms:4'-(4-iodo-benzoyloxy)-biphenyl-4-carboxylic acid nonyl ester

Chemical Property of 4'-(4-iodo-benzoyloxy)-biphenyl-4-carboxylic acid nonyl ester

Chemical Property:

Purity/Quality:

Safty Information:

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• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 4'-(4-iodo-benzoyloxy)-biphenyl-4-carboxylic acid nonyl ester

There total 3 articles about 4'-(4-iodo-benzoyloxy)-biphenyl-4-carboxylic acid nonyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

4-iodobenzoic acid (619-58-9) + 4'-Hydroxy-biphenyl-4-carboxylic acid nonyl ester (132328-88-2) → 4'-(4-iodo-benzoyloxy)-biphenyl-4-carboxylic acid nonyl ester (727668-65-7)

Guidance literature:

4-iodobenzoic acid; 4'-Hydroxy-biphenyl-4-carboxylic acid nonyl ester; With dicyclohexyl-carbodiimide; dmap; In dichloromethane; for 24h;

In dichloromethane; for 4h; Heating;

DOI:10.1080/15421400490425784

Reference yield:

1-Bromononane (693-58-3) → 4'-(4-iodo-benzoyloxy)-biphenyl-4-carboxylic acid nonyl ester (727668-65-7)

Guidance literature:

Multi-step reaction with 2 steps

1.1: 37.4 percent / KOH / dimethylsulfoxide / 48 h

2.1: DCC / DMAP / CH₂Cl₂ / 24 h

2.2: 73 percent / CH₂Cl₂ / 4 h / Heating

With potassium hydroxide; dicyclohexyl-carbodiimide; dmap; In dichloromethane; dimethyl sulfoxide;

DOI:10.1080/15421400490425784

Reference yield:

4'-Hydroxybiphenyl-4-carboxylic acid (58574-03-1) → 4'-(4-iodo-benzoyloxy)-biphenyl-4-carboxylic acid nonyl ester (727668-65-7)

Guidance literature:

Multi-step reaction with 2 steps

1.1: 37.4 percent / KOH / dimethylsulfoxide / 48 h

2.1: DCC / DMAP / CH₂Cl₂ / 24 h

2.2: 73 percent / CH₂Cl₂ / 4 h / Heating

With potassium hydroxide; dicyclohexyl-carbodiimide; dmap; In dichloromethane; dimethyl sulfoxide;

DOI:10.1080/15421400490425784

upstream raw materials:

4-iodobenzoic acid

4'-Hydroxy-biphenyl-4-carboxylic acid nonyl ester

1-Bromononane

4'-Hydroxybiphenyl-4-carboxylic acid

Refernces