allyl 2,4-di-O-benzyl-3-O-(3,4,6-tri-O-acetyl-2-(4,5-dichlorophthalimido)-2-deoxy-β-D-glucopyranosyl)-α-L-fucopyranoside

Base Information

• Chemical Name: allyl 2,4-di-O-benzyl-3-O-(3,4,6-tri-O-acetyl-2-(4,5-dichlorophthalimido)-2-deoxy-β-D-glucopyranosyl)-α-L-fucopyranoside
• CAS No.: 1245797-77-6
• Molecular Formula: C₄₃H₄₅Cl₂NO₁₄
• Molecular Weight: 870.735
• Mol file: 1245797-77-6.mol

Synonyms:allyl 2,4-di-O-benzyl-3-O-(3,4,6-tri-O-acetyl-2-(4,5-dichlorophthalimido)-2-deoxy-β-D-glucopyranosyl)-α-L-fucopyranoside

Chemical Property of allyl 2,4-di-O-benzyl-3-O-(3,4,6-tri-O-acetyl-2-(4,5-dichlorophthalimido)-2-deoxy-β-D-glucopyranosyl)-α-L-fucopyranoside

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of allyl 2,4-di-O-benzyl-3-O-(3,4,6-tri-O-acetyl-2-(4,5-dichlorophthalimido)-2-deoxy-β-D-glucopyranosyl)-α-L-fucopyranoside

There total 1 articles about allyl 2,4-di-O-benzyl-3-O-(3,4,6-tri-O-acetyl-2-(4,5-dichlorophthalimido)-2-deoxy-β-D-glucopyranosyl)-α-L-fucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

3,4,6-tri-O-acetyl-2-(4,5-dichlorophthalimido)-2-deoxy-D-glucopyranosyl bromide (1036637-16-7) + allyl 2,4-di-O-benzyl-α-L-fucopyranoside (62396-57-0) → allyl 2,4-di-O-benzyl-3-O-(3,4,6-tri-O-acetyl-2-(4,5-dichlorophthalimido)-2-deoxy-β-D-glucopyranosyl)-α-L-fucopyranoside (1245797-77-6)

Guidance literature:

With 2,4,6-trimethyl-pyridine; silver trifluoromethanesulfonate; In dichloromethane; toluene; at -30 ℃; for 1h; Inert atmosphere;

DOI:10.1021/ja105216u

Reference yield:

allyl 2,4-di-O-benzyl-3-O-(3,4,6-tri-O-acetyl-2-(4,5-dichlorophthalimido)-2-deoxy-β-D-glucopyranosyl)-α-L-fucopyranoside (1245797-77-6) → C35H45NO12

Guidance literature:

With methanol; ethylenediamine; Inert atmosphere;

DOI:10.1021/ja105216u

upstream raw materials:

3,4,6-tri-O-acetyl-2-(4,5-dichlorophthalimido)-2-deoxy-D-glucopyranosyl bromide

allyl 2,4-di-O-benzyl-α-L-fucopyranoside