N-<2-<4-(4-carboxy-1,3-thiazol-2-yl)-1,3-thiazol-2-yl>ethyl>-2-nitro-3-benzyloxy-4-methylbenzamide

Base Information

Chemical Name:N-<2-<4-(4-carboxy-1,3-thiazol-2-yl)-1,3-thiazol-2-yl>ethyl>-2-nitro-3-benzyloxy-4-methylbenzamide
CAS No.:159490-84-3
Molecular Formula:C₂₄H₂₀N₄O₆S₂
Molecular Weight:524.578
Hs Code.:

Synonyms:N-<2-<4-(4-carboxy-1,3-thiazol-2-yl)-1,3-thiazol-2-yl>ethyl>-2-nitro-3-benzyloxy-4-methylbenzamide

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Chemical Property of N-<2-<4-(4-carboxy-1,3-thiazol-2-yl)-1,3-thiazol-2-yl>ethyl>-2-nitro-3-benzyloxy-4-methylbenzamide

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Technology Process of N-<2-<4-(4-carboxy-1,3-thiazol-2-yl)-1,3-thiazol-2-yl>ethyl>-2-nitro-3-benzyloxy-4-methylbenzamide

There total 1 articles about N-<2-<4-(4-carboxy-1,3-thiazol-2-yl)-1,3-thiazol-2-yl>ethyl>-2-nitro-3-benzyloxy-4-methylbenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 7536-35-8
2-nitro-3-benzyloxy-4-methylbenzoyl chloride

: 30760-84-0
2-<2-(2-aminoethyl)-1,3-thiazol-4-yl>-1,3-thiazole-4-carboxylic acid

: 159490-84-3
N-<2-<4-(4-carboxy-1,3-thiazol-2-yl)-1,3-thiazol-2-yl>ethyl>-2-nitro-3-benzyloxy-4-methylbenzamide

Guidance literature:: With sodium hydroxide; In 1,4-dioxane; for 16h; Ambient temperature;

Reference yield: 90.0%

: 159490-84-3
N-<2-<4-(4-carboxy-1,3-thiazol-2-yl)-1,3-thiazol-2-yl>ethyl>-2-nitro-3-benzyloxy-4-methylbenzamide

: 159490-85-4
N-<2-<4-(4-chloroformyl-1,3-thiazol-2-yl)-1,3-thiazol-2-yl>ethyl>-2-nitro-3-benzyloxy-4-methylbenzamide

Guidance literature:: With thionyl chloride; In benzene; Heating;

Reference yield:

: 159490-84-3
N-<2-<4-(4-carboxy-1,3-thiazol-2-yl)-1,3-thiazol-2-yl>ethyl>-2-nitro-3-benzyloxy-4-methylbenzamide

: 2'-[2-(2-Amino-3-hydroxy-4-methyl-benzoylamino)-ethyl]-[2,4']bithiazolyl-4-carboxylic acid (3-dimethylamino-propyl)-amide; compound with trifluoro-acetic acid

Guidance literature:: Multi-step reaction with 4 steps

1: 90 percent / thionyl chloride / benzene / Heating

2: 83 percent / dioxane / a) 5-10 deg C, 1 h, b) 18-20 deg C, 15 h

3: 92 percent / 16 h / 18 - 20 °C

4: H₂ / Pd/C / ethanol

With thionyl chloride; hydrogen; palladium on activated charcoal; In 1,4-dioxane; ethanol; benzene;