Technology Process of C54H54N4Si2
There total 3 articles about C54H54N4Si2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
sodium t-butanolate;
tri-tert-butyl phosphine; palladium diacetate;
In
toluene;
at 85 ℃;
for 7h;
Inert atmosphere;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: potassium carbonate / copper(l) iodide; N,N`-dimethylethylenediamine / xylene / 18 h / Inert atmosphere; Reflux
2: potassium hydroxide; water / toluene; ethanol / 8 h / Reflux
3: sodium t-butanolate / palladium diacetate; tri-tert-butyl phosphine / toluene / 7 h / 85 °C / Inert atmosphere
With
water; potassium carbonate; potassium hydroxide; sodium t-butanolate;
copper(l) iodide; tri-tert-butyl phosphine; palladium diacetate; N,N`-dimethylethylenediamine;
In
ethanol; toluene; xylene;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: potassium carbonate / copper(l) iodide; N,N`-dimethylethylenediamine / xylene / 18 h / Inert atmosphere; Reflux
2: potassium carbonate / copper(l) iodide; N,N`-dimethylethylenediamine / xylene / 18 h / Inert atmosphere; Reflux
3: potassium hydroxide; water / toluene; ethanol / 8 h / Reflux
4: sodium t-butanolate / palladium diacetate; tri-tert-butyl phosphine / toluene / 7 h / 85 °C / Inert atmosphere
With
water; potassium carbonate; potassium hydroxide; sodium t-butanolate;
copper(l) iodide; tri-tert-butyl phosphine; palladium diacetate; N,N`-dimethylethylenediamine;
In
ethanol; toluene; xylene;