diethyl 3,4-bis(4-(decyloxy)-3-methoxybenzyloxy)thiophene-2,5-dicarboxylate

Base Information

Chemical Name:diethyl 3,4-bis(4-(decyloxy)-3-methoxybenzyloxy)thiophene-2,5-dicarboxylate
CAS No.:1447240-15-4
Molecular Formula:C₄₆H₆₈O₁₀S
Molecular Weight:813.106
Hs Code.:

Synonyms:diethyl 3,4-bis(4-(decyloxy)-3-methoxybenzyloxy)thiophene-2,5-dicarboxylate

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Chemical Property of diethyl 3,4-bis(4-(decyloxy)-3-methoxybenzyloxy)thiophene-2,5-dicarboxylate

Chemical Property:

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Technology Process of diethyl 3,4-bis(4-(decyloxy)-3-methoxybenzyloxy)thiophene-2,5-dicarboxylate

There total 5 articles about diethyl 3,4-bis(4-(decyloxy)-3-methoxybenzyloxy)thiophene-2,5-dicarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1407239-97-7
C₁₈H₂₉BrO₂

: 1822-66-8
3,4-dihydroxythiophene-2,5-dicarboxylic acid diethyl ester

: 1447240-15-4
diethyl 3,4-bis(4-(decyloxy)-3-methoxybenzyloxy)thiophene-2,5-dicarboxylate

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 60 ℃; for 8h;
DOI:10.1007/s12039-013-0366-1

Reference yield:

: 121-33-5,8014-42-4
vanillin

: 1447240-15-4
diethyl 3,4-bis(4-(decyloxy)-3-methoxybenzyloxy)thiophene-2,5-dicarboxylate

Guidance literature:: Multi-step reaction with 4 steps

1: potassium carbonate / N,N-dimethyl-formamide / 60 °C

2: sodium tetrahydroborate / methanol / 2 h / 20 °C

3: phosphorus tribromide / diethyl ether / 5 h / 20 °C

4: potassium carbonate / N,N-dimethyl-formamide / 8 h / 60 °C

With sodium tetrahydroborate; phosphorus tribromide; potassium carbonate; In methanol; diethyl ether; N,N-dimethyl-formamide;
DOI:10.1007/s12039-013-0366-1

Reference yield:

: 1409278-30-3
(4-decyloxy-3-methoxyphenyl)methanol

: 1447240-15-4
diethyl 3,4-bis(4-(decyloxy)-3-methoxybenzyloxy)thiophene-2,5-dicarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: phosphorus tribromide / diethyl ether / 5 h / 20 °C

2: potassium carbonate / N,N-dimethyl-formamide / 8 h / 60 °C

With phosphorus tribromide; potassium carbonate; In diethyl ether; N,N-dimethyl-formamide;
DOI:10.1007/s12039-013-0366-1