5-((2S,3S,4R,5S,6S)-3,4,5-Trihydroxy-6-methyl-tetrahydro-pyran-2-ylsulfanylmethyl)-isophthalic acid monoethyl ester

Base Information

Chemical Name:5-((2S,3S,4R,5S,6S)-3,4,5-Trihydroxy-6-methyl-tetrahydro-pyran-2-ylsulfanylmethyl)-isophthalic acid monoethyl ester
CAS No.:374678-25-8
Molecular Formula:C₁₇H₂₂O₈S
Molecular Weight:386.423
Hs Code.:

Synonyms:5-((2S,3S,4R,5S,6S)-3,4,5-Trihydroxy-6-methyl-tetrahydro-pyran-2-ylsulfanylmethyl)-isophthalic acid monoethyl ester

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Chemical Property of 5-((2S,3S,4R,5S,6S)-3,4,5-Trihydroxy-6-methyl-tetrahydro-pyran-2-ylsulfanylmethyl)-isophthalic acid monoethyl ester

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Technology Process of 5-((2S,3S,4R,5S,6S)-3,4,5-Trihydroxy-6-methyl-tetrahydro-pyran-2-ylsulfanylmethyl)-isophthalic acid monoethyl ester

There total 3 articles about 5-((2S,3S,4R,5S,6S)-3,4,5-Trihydroxy-6-methyl-tetrahydro-pyran-2-ylsulfanylmethyl)-isophthalic acid monoethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 374678-24-7
5-((2S,3S,4R,5S,6S)-3,4,5-Trihydroxy-6-methyl-tetrahydro-pyran-2-ylsulfanylmethyl)-isophthalic acid diethyl ester

: 374678-25-8
5-((2S,3S,4R,5S,6S)-3,4,5-Trihydroxy-6-methyl-tetrahydro-pyran-2-ylsulfanylmethyl)-isophthalic acid monoethyl ester

Guidance literature:: With potassium hydroxide; In ethanol;
DOI:10.1016/S0960-894X(01)00430-9

Reference yield:

: 156750-11-7
5-(bromomethyl)isophthalic acid diethyl ester

: 374678-25-8
5-((2S,3S,4R,5S,6S)-3,4,5-Trihydroxy-6-methyl-tetrahydro-pyran-2-ylsulfanylmethyl)-isophthalic acid monoethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 92 percent / 20 percent NaOEt / ethanol

2: 90 percent / KOH / ethanol

With potassium hydroxide; sodium ethanolate; In ethanol;
DOI:10.1016/S0960-894X(01)00430-9

Reference yield:

: 181425-91-2
diethyl 5-(hydroxymethyl)isophthalate

: 374678-25-8
5-((2S,3S,4R,5S,6S)-3,4,5-Trihydroxy-6-methyl-tetrahydro-pyran-2-ylsulfanylmethyl)-isophthalic acid monoethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 83 percent / PPh₃; CBr₄ / CH₂Cl₂

2: 92 percent / 20 percent NaOEt / ethanol

3: 90 percent / KOH / ethanol

With potassium hydroxide; carbon tetrabromide; sodium ethanolate; triphenylphosphine; In ethanol; dichloromethane;
DOI:10.1016/S0960-894X(01)00430-9