4-methoxyphenyl O-[(methyl 2,3,4-tri-O-(4-methylbenzoyl)-β-D-glucopyranosid)uronate]-(1->3)-O-(2,4,6-tri-O-acetyl-β-D-galactopyranosyl)-(1->3)-O-(2,4,6-tri-O-acetyl-β-D-galactopyranosyl)-(1->4)-2,3-di-O-(4-methylbenzoyl)-β-D-xylopyranoside

Base Information

• Chemical Name: 4-methoxyphenyl O-[(methyl 2,3,4-tri-O-(4-methylbenzoyl)-β-D-glucopyranosid)uronate]-(1->3)-O-(2,4,6-tri-O-acetyl-β-D-galactopyranosyl)-(1->3)-O-(2,4,6-tri-O-acetyl-β-D-galactopyranosyl)-(1->4)-2,3-di-O-(4-methylbenzoyl)-β-D-xylopyranoside
• CAS No.: 943977-41-1
• Molecular Formula: C₈₃H₈₈O₃₃
• Molecular Weight: 1613.59

Synonyms:4-methoxyphenyl O-[(methyl 2,3,4-tri-O-(4-methylbenzoyl)-β-D-glucopyranosid)uronate]-(1->3)-O-(2,4,6-tri-O-acetyl-β-D-galactopyranosyl)-(1->3)-O-(2,4,6-tri-O-acetyl-β-D-galactopyranosyl)-(1->4)-2,3-di-O-(4-methylbenzoyl)-β-D-xylopyranoside

Chemical Property of 4-methoxyphenyl O-[(methyl 2,3,4-tri-O-(4-methylbenzoyl)-β-D-glucopyranosid)uronate]-(1->3)-O-(2,4,6-tri-O-acetyl-β-D-galactopyranosyl)-(1->3)-O-(2,4,6-tri-O-acetyl-β-D-galactopyranosyl)-(1->4)-2,3-di-O-(4-methylbenzoyl)-β-D-xylopyranoside

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Technology Process of 4-methoxyphenyl O-[(methyl 2,3,4-tri-O-(4-methylbenzoyl)-β-D-glucopyranosid)uronate]-(1->3)-O-(2,4,6-tri-O-acetyl-β-D-galactopyranosyl)-(1->3)-O-(2,4,6-tri-O-acetyl-β-D-galactopyranosyl)-(1->4)-2,3-di-O-(4-methylbenzoyl)-β-D-xylopyranoside

There total 1 articles about 4-methoxyphenyl O-[(methyl 2,3,4-tri-O-(4-methylbenzoyl)-β-D-glucopyranosid)uronate]-(1->3)-O-(2,4,6-tri-O-acetyl-β-D-galactopyranosyl)-(1->3)-O-(2,4,6-tri-O-acetyl-β-D-galactopyranosyl)-(1->4)-2,3-di-O-(4-methylbenzoyl)-β-D-xylopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 31.0%

(2S,3S,4S,5R,6S)-3,4,5-Tris-(4-methyl-benzoyloxy)-6-methylsulfanyl-tetrahydro-pyran-2-carboxylic acid methyl ester + 4-methoxyphenyl O-(2,4,6-tri-O-acetyl-β-D-galactopyranosyl)-(1->3)-O-(2,4,6-tri-O-acetyl-β-D-galactopyranosyl)-(1->4)-2,3-di-O-(4-methylbenzoyl)-β-D-xylopyranoside (475101-62-3) → 4-methoxyphenyl O-[(methyl 2,3,4-tri-O-(4-methylbenzoyl)-β-D-glucopyranosid)uronate]-(1->3)-O-(2,4,6-tri-O-acetyl-β-D-galactopyranosyl)-(1->3)-O-(2,4,6-tri-O-acetyl-β-D-galactopyranosyl)-(1->4)-2,3-di-O-(4-methylbenzoyl)-β-D-xylopyranoside (943977-41-1)

Guidance literature:

With tetrabutylammomium bromide; silver trifluoromethanesulfonate; copper(ll) bromide; In chloroform;

DOI:10.1016/S0960-894X(02)00327-X

Reference yield: 93.0%

4-methoxyphenyl O-[(methyl 2,3,4-tri-O-(4-methylbenzoyl)-β-D-glucopyranosid)uronate]-(1->3)-O-(2,4,6-tri-O-acetyl-β-D-galactopyranosyl)-(1->3)-O-(2,4,6-tri-O-acetyl-β-D-galactopyranosyl)-(1->4)-2,3-di-O-(4-methylbenzoyl)-β-D-xylopyranoside (943977-41-1) → C76H82O32

Guidance literature:

With ammonium cerium(IV) nitrate; In water; acetonitrile; at 0 ℃; for 4.5h;

DOI:10.1080/07328300701296810

Reference yield:

4-methoxyphenyl O-[(methyl 2,3,4-tri-O-(4-methylbenzoyl)-β-D-glucopyranosid)uronate]-(1->3)-O-(2,4,6-tri-O-acetyl-β-D-galactopyranosyl)-(1->3)-O-(2,4,6-tri-O-acetyl-β-D-galactopyranosyl)-(1->4)-2,3-di-O-(4-methylbenzoyl)-β-D-xylopyranoside (943977-41-1) → C76H82O32

Guidance literature:

With ammonium cerium(IV) nitrate; water; In acetonitrile;

DOI:10.1016/S0960-894X(02)00327-X

upstream raw materials:

4-methoxyphenyl O-(2,4,6-tri-O-acetyl-β-D-galactopyranosyl)-(1->3)-O-(2,4,6-tri-O-acetyl-β-D-galactopyranosyl)-(1->4)-2,3-di-O-(4-methylbenzoyl)-β-D-xylopyranoside

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