(1R,2S)-2-Methanesulfonylaminocarbonyl-cyclobutanecarboxylic acid isopropyl ester

Base Information

Chemical Name:(1R,2S)-2-Methanesulfonylaminocarbonyl-cyclobutanecarboxylic acid isopropyl ester
CAS No.:180790-22-1
Molecular Formula:C₁₀H₁₇NO₅S
Molecular Weight:263.315
Hs Code.:

Synonyms:(1R,2S)-2-Methanesulfonylaminocarbonyl-cyclobutanecarboxylic acid isopropyl ester

Suppliers and Price of (1R,2S)-2-Methanesulfonylaminocarbonyl-cyclobutanecarboxylic acid isopropyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (1R,2S)-2-Methanesulfonylaminocarbonyl-cyclobutanecarboxylic acid isopropyl ester

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (1R,2S)-2-Methanesulfonylaminocarbonyl-cyclobutanecarboxylic acid isopropyl ester

There total 1 articles about (1R,2S)-2-Methanesulfonylaminocarbonyl-cyclobutanecarboxylic acid isopropyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 4462-96-8
cis-1,2-cyclobutane dicarboxylic anhydride

: 180790-22-1
(1R,2S)-2-Methanesulfonylaminocarbonyl-cyclobutanecarboxylic acid isopropyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 72 percent / NH₄Cl, AcONa / acetic acid / 72 h / Heating

2: 1.) Et₃N / 1.) MeCN, 0 degC, 10 min; 2.) MeCN, 2.5 h

3: 1.) (2-naphthyl)-substituted TADDOL / 1.) Et₂O, r.t., 3 h; 2.) THF, -30 degC, 7 d

With (2-naphthyl)-substituted TADDOL; sodium acetate; ammonium chloride; triethylamine; In acetic acid;
DOI:10.1002/hlca.19960790328

Reference yield:

: 180790-22-1
(1R,2S)-2-Methanesulfonylaminocarbonyl-cyclobutanecarboxylic acid isopropyl ester

: (S)-3,3,3-Trifluoro-2-methoxy-2-phenyl-propionic acid (1R,2S)-2-(methanesulfonylamino-methyl)-cyclobutylmethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 97 percent / LiAlH₄ / diethyl ether / 0.5 h / 0 °C

2: 4-(dimethylamino)pyridine / CDCl₃

With dmap; lithium aluminium tetrahydride; In diethyl ether; chloroform-d1;
DOI:10.1002/hlca.19960790328

Reference yield:

: 180790-22-1
(1R,2S)-2-Methanesulfonylaminocarbonyl-cyclobutanecarboxylic acid isopropyl ester

: (R)-3,3,3-Trifluoro-2-methoxy-2-phenyl-propionic acid (1R,2S)-2-(methanesulfonylamino-methyl)-cyclobutylmethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 97 percent / LiAlH₄ / diethyl ether / 0.5 h / 0 °C

2: 4-(dimethylamino)pyridine / CDCl₃

With dmap; lithium aluminium tetrahydride; In diethyl ether; chloroform-d1;
DOI:10.1002/hlca.19960790328