benzyl (6-benzyloxycarbonylaminohexyl) 2,3,5,6-O-tetrakis(benzyloxymethyl)-D-myo-insit-1-yl phosphate 4-(dibenzyl phosphate)

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Chemical Name:benzyl (6-benzyloxycarbonylaminohexyl) 2,3,5,6-O-tetrakis(benzyloxymethyl)-D-myo-insit-1-yl phosphate 4-(dibenzyl phosphate)
CAS No.:1188371-74-5
Molecular Formula:C₇₃H₈₃NO₁₈P₂
Molecular Weight:1324.41
Hs Code.:

Synonyms:benzyl (6-benzyloxycarbonylaminohexyl) 2,3,5,6-O-tetrakis(benzyloxymethyl)-D-myo-insit-1-yl phosphate 4-(dibenzyl phosphate)

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Chemical Property of benzyl (6-benzyloxycarbonylaminohexyl) 2,3,5,6-O-tetrakis(benzyloxymethyl)-D-myo-insit-1-yl phosphate 4-(dibenzyl phosphate)

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Technology Process of benzyl (6-benzyloxycarbonylaminohexyl) 2,3,5,6-O-tetrakis(benzyloxymethyl)-D-myo-insit-1-yl phosphate 4-(dibenzyl phosphate)

There total 2 articles about benzyl (6-benzyloxycarbonylaminohexyl) 2,3,5,6-O-tetrakis(benzyloxymethyl)-D-myo-insit-1-yl phosphate 4-(dibenzyl phosphate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 1188371-72-3
2,3,5,6-O-tetrakis(benzyloxymethyl)-D-myo-insitol 4-(dibenzyl phosphate)

: benzyl N-Cbz-6-aminohexyl diisopropylphosphoramidite

: 1188371-74-5
benzyl (6-benzyloxycarbonylaminohexyl) 2,3,5,6-O-tetrakis(benzyloxymethyl)-D-myo-insit-1-yl phosphate 4-(dibenzyl phosphate)

Guidance literature:: 2,3,5,6-O-tetrakis(benzyloxymethyl)-D-myo-insitol 4-(dibenzyl phosphate); benzyl N-Cbz-6-aminohexyl diisopropylphosphoramidite; With 1H-tetrazole; In dichloromethane; acetonitrile; at 20 ℃; for 18h; Inert atmosphere;

With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; acetonitrile; at -60 - 20 ℃;
DOI:10.1002/ejoc.200900476

Reference yield:

: C₇₃H₈₃NO₁₇P₂

: 1188371-74-5
benzyl (6-benzyloxycarbonylaminohexyl) 2,3,5,6-O-tetrakis(benzyloxymethyl)-D-myo-insit-1-yl phosphate 4-(dibenzyl phosphate)

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; acetonitrile; at -60 ℃; for 1h;
DOI:10.1016/j.chembiol.2011.07.022

Reference yield: 100.0%

: 1188371-74-5
benzyl (6-benzyloxycarbonylaminohexyl) 2,3,5,6-O-tetrakis(benzyloxymethyl)-D-myo-insit-1-yl phosphate 4-(dibenzyl phosphate)

: 1-(6-aminohexyl sodium phosphate)-D-myo-insitol 4-(disodium phosphate)

Guidance literature:: benzyl (6-benzyloxycarbonylaminohexyl) 2,3,5,6-O-tetrakis(benzyloxymethyl)-D-myo-insit-1-yl phosphate 4-(dibenzyl phosphate); With Pearlman catalyst; hydrogen; In methanol; at 20 ℃; for 72h; under 760.051 Torr;

In water; for 3h;
DOI:10.1002/ejoc.200900476