[(WAY₁-Cp)Re(CO)3]

Base Information

• Chemical Name: [(WAY₁-Cp)Re(CO)3]
• CAS No.: 374929-96-1
• Molecular Formula: C₂₁H₂₁N₂O₅Re
• Molecular Weight: 567.615

Synonyms:[(WAY₁-Cp)Re(CO)3]

Chemical Property of [(WAY₁-Cp)Re(CO)3]

Chemical Property:

Purity/Quality:

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Technology Process of [(WAY₁-Cp)Re(CO)3]

There total 2 articles about [(WAY₁-Cp)Re(CO)3] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 23.0%

(NEt4)2[rhenium(I)(bromide)3(carbonyl)3] + Na[(WAY1-Cp)] → [(WAY1-Cp)Re(CO)3] (374929-96-1)

Guidance literature:

With phosphate buffer; In water; (NEt4)2(ReBr3(CO)3) in phosphate buffer added dropwise over 2 h to soln. of cyclopentadiene derivative in phosphate buffer, mixt. heated (3 h, 75 °C); ppt. filtered, dissolved in CH2Cl2, sepd. by chromy., recrystd. from acidic EtOH/H2O mixt.;

DOI:10.1002/1521-3773(20010817)40:16<3062::AID-ANIE3062>3.0.CO;2-O

Reference yield: 15.0%

rhenium(I) pentacarbonyl bromide (14220-21-4) + Na[(WAY1-Cp)] → [(WAY1-Cp)Re(CO)3] (374929-96-1)

Guidance literature:

In benzene; using Schlenk techniques; by a react. of Re-contg. compd. with a ligand in benzene overnight; evapn. of the solvent; the residue was washed with water and extd. with hexane and purified by silica gel chromy. (3:1 CH2Cl2-hexane); HPLC; (1)H NMR spectra monitoring;

DOI:10.1021/ic0204575

upstream raw materials:

rhenium(I) pentacarbonyl bromide

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