2-(1-Chlorocyclopropyl)-1-(2-chlorophenyl)-3-hydrazinylpropan-2-ol

Base Information

• Chemical Name: 2-(1-Chlorocyclopropyl)-1-(2-chlorophenyl)-3-hydrazinylpropan-2-ol
• CAS No.: 222408-91-5
• Molecular Formula: C₁₂H₁₆Cl₂N₂O
• Molecular Weight: 275.178
• DSSTox Substance ID: DTXSID601335317

Synonyms:2-(1-chlorocyclopropyl)-1-(2-chlorophenyl)-3-hydrazinylpropan-2-ol;222408-91-5;SCHEMBL6572716;DTXSID601335317

Chemical Property of 2-(1-Chlorocyclopropyl)-1-(2-chlorophenyl)-3-hydrazinylpropan-2-ol

Chemical Property:

• XLogP3: 1.8
• Hydrogen Bond Donor Count: 3
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 5
• Exact Mass: 274.0639685
• Heavy Atom Count: 17
• Complexity: 273

Purity/Quality:

98% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Canonical SMILES: C1CC1(C(CC2=CC=CC=C2Cl)(CNN)O)Cl

Technology Process of 2-(1-Chlorocyclopropyl)-1-(2-chlorophenyl)-3-hydrazinylpropan-2-ol

There total 4 articles about 2-(1-Chlorocyclopropyl)-1-(2-chlorophenyl)-3-hydrazinylpropan-2-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.4%

3-chloro-2-(1-chloro-cycloprop-1-yl)-1-(2-chloro-phenyl)-propan-2-ol → [2-(1-chloro-cycloprop-1-yl)-3-(2-chlorophenyl)-2-hydroxy]-propyl-1-hydrazine (222408-91-5)

Guidance literature:

With tetrabutylammomium bromide; hydrazine hydrate; sodium hydroxide; In ethanol; at 80 - 85 ℃; for 2h; Reagent/catalyst; Solvent; Temperature;

Reference yield: 91.0%

2-(1-chloro-cycloprop-1-yl)-2-(2'-chloro-benzyl)-oxirane → [2-(1-chloro-cycloprop-1-yl)-3-(2-chlorophenyl)-2-hydroxy]-propyl-1-hydrazine (222408-91-5)

Guidance literature:

With hydrazine hydrate; potassium carbonate; In tetrahydrofuran; at 15 - 70 ℃; for 5h; Reagent/catalyst; Solvent; Temperature;

Reference yield: 86.8%

3-chloro-2-(1-chloro-cycloprop-1-yl)-1-(2-chloro-phenyl)-propan-2-ol → [2-(1-chloro-cycloprop-1-yl)-3-(2-chlorophenyl)-2-hydroxy]-propyl-1-hydrazine (222408-91-5)

Guidance literature:

With hydrazine; at 100 ℃; for 5h; Under N₂;

upstream raw materials:

1-(1-chlorocyclopropyl)-2-(2-chlorophenyl)ethanone

Downstream raw materials:

[2-(1-chlorocyclopropyl-1-yl)-1-(2-chlorophenyl)-2-hydroxy-3-propane]-(1,2,4-triazolidine-3-thiol-1-yl)

C₁₆H₂₁Cl₂N₃OS

2?[(2RS)?2?(1?chlorocyclopropyl)?3?(2?chlorophenyl)?2?hydroxypropyl]?2H?1,2,4?triazole?3(4H)?thione

prothioconazole

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