(1R,2S,6R,7R)-3-Oxo-5,6-diphenyl-8-aza-tricyclo[5.3.2.0^2,6]dodeca-4,9,11-triene-2,4,8-tricarboxylic acid triethyl ester

Base Information

• Chemical Name: (1R,2S,6R,7R)-3-Oxo-5,6-diphenyl-8-aza-tricyclo[5.3.2.0^2,6]dodeca-4,9,11-triene-2,4,8-tricarboxylic acid triethyl ester
• CAS No.: 77940-53-5
• Molecular Formula: C₃₂H₃₁NO₇
• Molecular Weight: 541.601

Synonyms:(1R,2S,6R,7R)-3-Oxo-5,6-diphenyl-8-aza-tricyclo[5.3.2.0^2,6]dodeca-4,9,11-triene-2,4,8-tricarboxylic acid triethyl ester

Chemical Property of (1R,2S,6R,7R)-3-Oxo-5,6-diphenyl-8-aza-tricyclo[5.3.2.0^2,6]dodeca-4,9,11-triene-2,4,8-tricarboxylic acid triethyl ester

Chemical Property:

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Technology Process of (1R,2S,6R,7R)-3-Oxo-5,6-diphenyl-8-aza-tricyclo[5.3.2.0^2,6]dodeca-4,9,11-triene-2,4,8-tricarboxylic acid triethyl ester

There total 1 articles about (1R,2S,6R,7R)-3-Oxo-5,6-diphenyl-8-aza-tricyclo[5.3.2.0^2,6]dodeca-4,9,11-triene-2,4,8-tricarboxylic acid triethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

diethyl 2-oxo-4,5-diphenylcyclopenta-3,5-diene-1,3-dicarboxylate (57558-10-8) + N-ethoxycarbonylazepine (2955-79-5) → (1R,2S,6R,7R)-3-Oxo-5,6-diphenyl-8-aza-tricyclo[5.3.2.02,6]dodeca-4,9,11-triene-2,4,8-tricarboxylic acid triethyl ester (77940-53-5)

Guidance literature:

DOI:10.1021/ja00399a029

Reference yield: 97.0%

(1R,2S,6R,7R)-3-Oxo-5,6-diphenyl-8-aza-tricyclo[5.3.2.02,6]dodeca-4,9,11-triene-2,4,8-tricarboxylic acid triethyl ester (77940-53-5) → C32H31NO7 (77920-76-4)

Guidance literature:

In benzene; for 0.333333h; Ambient temperature; Irradiation;

DOI:10.1021/ja00399a029

upstream raw materials:

diethyl 2-oxo-4,5-diphenylcyclopenta-3,5-diene-1,3-dicarboxylate

N-ethoxycarbonylazepine

Downstream raw materials:

C₃₂H₃₁NO₇

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