{4-[4-(3,3-dimethyl-2,4-dioxo-azetidin-1-yl)-benzyl]-phenyl}-carbamic acid decyl ester

Base Information

• Chemical Name: {4-[4-(3,3-dimethyl-2,4-dioxo-azetidin-1-yl)-benzyl]-phenyl}-carbamic acid decyl ester
• CAS No.: 900503-07-3
• Molecular Formula: C₂₉H₃₈N₂O₄
• Molecular Weight: 478.632
• Mol file: 900503-07-3.mol

Synonyms:{4-[4-(3,3-dimethyl-2,4-dioxo-azetidin-1-yl)-benzyl]-phenyl}-carbamic acid decyl ester

Chemical Property of {4-[4-(3,3-dimethyl-2,4-dioxo-azetidin-1-yl)-benzyl]-phenyl}-carbamic acid decyl ester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of {4-[4-(3,3-dimethyl-2,4-dioxo-azetidin-1-yl)-benzyl]-phenyl}-carbamic acid decyl ester

There total 1 articles about {4-[4-(3,3-dimethyl-2,4-dioxo-azetidin-1-yl)-benzyl]-phenyl}-carbamic acid decyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

di(4-isocyanatophenyl)methane (101-68-8,25686-28-6,97568-33-7) → {4-[4-(3,3-dimethyl-2,4-dioxo-azetidin-1-yl)-benzyl]-phenyl}-carbamic acid decyl ester (900503-07-3)

Guidance literature:

Multi-step reaction with 2 steps

1: 33 percent / Et₃N / xylene / 7 h / Heating

2: 95 percent / tetrahydrofuran / 3 h / 80 °C

With triethylamine; In tetrahydrofuran; xylene;

DOI:10.1039/b600544f

Reference yield: 95.0%

{4-[4-(3,3-dimethyl-2,4-dioxo-azetidin-1-yl)-benzyl]-phenyl}-carbamic acid decyl ester (900503-07-3) + 3-azapentane-1,5-diamine (111-40-0,98824-35-2) → C62H89N7O8

Guidance literature:

In tetrahydrofuran; at 60 ℃; for 2h;

DOI:10.1039/b600544f

upstream raw materials:

di(4-isocyanatophenyl)methane