C₂₂H₂₇NO₃S

Base Information

• Chemical Name: C₂₂H₂₇NO₃S
• CAS No.: 1370290-70-2
• Molecular Formula: C₂₂H₂₇NO₃S
• Molecular Weight: 385.527
• Mol file: 1370290-70-2.mol

Synonyms:C₂₂H₂₇NO₃S

Chemical Property of C₂₂H₂₇NO₃S

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₂H₂₇NO₃S

There total 1 articles about C₂₂H₂₇NO₃S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

C24H31NO4S (1370290-67-7) → C22H27NO3S (1370290-70-2)

Guidance literature:

With tetrafluoroboric acid; In water; acetonitrile; at 60 ℃; for 48h;

DOI:10.1021/ol300571b

Reference yield:

C22H27NO3S (1370290-70-2) → C22H25NO3S

Guidance literature:

With Dess-Martin periodane; In dichloromethane; at 0 - 20 ℃; for 3h;

DOI:10.1021/ol300571b

Reference yield:

C22H27NO3S (1370290-70-2) → C23H29NO2S (1370290-71-3)

Guidance literature:

Multi-step reaction with 3 steps

1: Dess-Martin periodane / dichloromethane / 3 h / 0 - 20 °C

2: tetrahydrofuran / 2 h / 0 °C

3: palladium 10% on activated carbon; hydrogen / ethyl acetate / 2 h / 20 °C / 760.05 Torr

With palladium 10% on activated carbon; hydrogen; Dess-Martin periodane; In tetrahydrofuran; dichloromethane; ethyl acetate;

DOI:10.1021/ol300571b

upstream raw materials:

C₂₄H₃₁NO₄S

Downstream raw materials:

C₂₃H₂₉NO₂S

C₂₅H₃₁NO₂S