diallyl [phenyl 2-acetamido-3-O-benzoyl-2,4-dideoxy-β-L-threo-hex-4-enopyranoside-6-yl]-phosphonate

Base Information

Chemical Name:diallyl [phenyl 2-acetamido-3-O-benzoyl-2,4-dideoxy-β-L-threo-hex-4-enopyranoside-6-yl]-phosphonate
CAS No.:404579-63-1
Molecular Formula:C₂₇H₃₀NO₉P
Molecular Weight:543.51
Hs Code.:

Synonyms:diallyl [phenyl 2-acetamido-3-O-benzoyl-2,4-dideoxy-β-L-threo-hex-4-enopyranoside-6-yl]-phosphonate

Suppliers and Price of diallyl [phenyl 2-acetamido-3-O-benzoyl-2,4-dideoxy-β-L-threo-hex-4-enopyranoside-6-yl]-phosphonate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of diallyl [phenyl 2-acetamido-3-O-benzoyl-2,4-dideoxy-β-L-threo-hex-4-enopyranoside-6-yl]-phosphonate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of diallyl [phenyl 2-acetamido-3-O-benzoyl-2,4-dideoxy-β-L-threo-hex-4-enopyranoside-6-yl]-phosphonate

There total 4 articles about diallyl [phenyl 2-acetamido-3-O-benzoyl-2,4-dideoxy-β-L-threo-hex-4-enopyranoside-6-yl]-phosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 404579-55-1
phenyl 2-acetamido-6-O-tert-butyldimethylsilyl-2-deoxy-β-D-glucopyranoside

: 404579-63-1
diallyl [phenyl 2-acetamido-3-O-benzoyl-2,4-dideoxy-β-L-threo-hex-4-enopyranoside-6-yl]-phosphonate

Guidance literature:: Multi-step reaction with 4 steps

1: 93 percent / pyridine / 1.33 h / -15 °C

2: 78 percent / acetyl chloride / methanol; diethyl ether / 0.33 h / 0 °C

3: 84 percent / phosphoric acid; pyridine; DCC / toluene; dimethylsulfoxide / 72 h / 20 °C

4: 100 percent / triethylamine / CH₂Cl₂ / 1.5 h / 20 °C

With pyridine; phosphoric acid; triethylamine; acetyl chloride; dicyclohexyl-carbodiimide; In methanol; diethyl ether; dichloromethane; dimethyl sulfoxide; toluene; 3: Pfitzner-Morffatt oxidation;
DOI:10.1021/ja017370n

Reference yield:

: 404579-59-5
phenyl 2-acetamido-3,4-di-O-benzoyl-2-deoxy-β-D-glucopyranoside

: 404579-63-1
diallyl [phenyl 2-acetamido-3-O-benzoyl-2,4-dideoxy-β-L-threo-hex-4-enopyranoside-6-yl]-phosphonate

Guidance literature:: Multi-step reaction with 2 steps

1: 84 percent / phosphoric acid; pyridine; DCC / toluene; dimethylsulfoxide / 72 h / 20 °C

2: 100 percent / triethylamine / CH₂Cl₂ / 1.5 h / 20 °C

With pyridine; phosphoric acid; triethylamine; dicyclohexyl-carbodiimide; In dichloromethane; dimethyl sulfoxide; toluene; 1: Pfitzner-Morffatt oxidation;
DOI:10.1021/ja017370n

Reference yield:

: 404579-57-3
phenyl 2-acetamido-3,4-di-O-benzoyl-6-O-tertbutyldimethylsilyl-2-deoxy-β-D-glucopyranoside

: 404579-63-1
diallyl [phenyl 2-acetamido-3-O-benzoyl-2,4-dideoxy-β-L-threo-hex-4-enopyranoside-6-yl]-phosphonate

Guidance literature:: Multi-step reaction with 3 steps

1: 78 percent / acetyl chloride / methanol; diethyl ether / 0.33 h / 0 °C

2: 84 percent / phosphoric acid; pyridine; DCC / toluene; dimethylsulfoxide / 72 h / 20 °C

3: 100 percent / triethylamine / CH₂Cl₂ / 1.5 h / 20 °C

With pyridine; phosphoric acid; triethylamine; acetyl chloride; dicyclohexyl-carbodiimide; In methanol; diethyl ether; dichloromethane; dimethyl sulfoxide; toluene; 2: Pfitzner-Morffatt oxidation;
DOI:10.1021/ja017370n