C₃₂H₄₉NO₄S

Base Information

Chemical Name:C₃₂H₄₉NO₄S
CAS No.:1365757-11-4
Molecular Formula:C₃₂H₄₉NO₄S
Molecular Weight:543.811
Hs Code.:

C<sub>32</sub>H<sub>49</sub>NO<sub>4</sub>S

Synonyms:C₃₂H₄₉NO₄S

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Chemical Property of C₃₂H₄₉NO₄S

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Technology Process of C₃₂H₄₉NO₄S

There total 8 articles about C₃₂H₄₉NO₄S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1365757-10-3
C₃₅H₅₃NO₄S

: 1365757-11-4
C₃₂H₄₉NO₄S

Guidance literature:: With camphor-10-sulfonic acid; In methanol; at 20 ℃;
DOI:10.1016/j.tetlet.2012.02.066

Reference yield:

: 916159-68-7
(2S,3S,4R)-2-azido-1-(tert-butyldiphenylsilyloxy)octadecane-3,4-diol

: 1365757-11-4
C₃₂H₄₉NO₄S

Guidance literature:: Multi-step reaction with 7 steps

1: toluene-4-sulfonic acid / dichloromethane / 20 °C

2: tetrabutyl ammonium fluoride / tetrahydrofuran / 20 °C

3: triethylamine / tetrahydrofuran / 0 - 20 °C

4: N-ethyl-N,N-diisopropylamine; triphenylphosphine / tetrahydrofuran; water / 60 °C

5: triethylamine / dichloromethane / 0 - 20 °C / Inert atmosphere

6: 1,8-diazabicyclo[5.4.0]undec-7-ene / acetonitrile / 0.08 h / 100 °C / 5171.77 Torr / Inert atmosphere; CEM Discover Focused_.(TM). Microwave reactor; Sealed vessel

7: camphor-10-sulfonic acid / methanol / 20 °C

With camphor-10-sulfonic acid; tetrabutyl ammonium fluoride; toluene-4-sulfonic acid; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; N-ethyl-N,N-diisopropylamine; triphenylphosphine; In tetrahydrofuran; methanol; dichloromethane; water; acetonitrile; 4: Staudinger reduction;
DOI:10.1016/j.tetlet.2012.02.066

Reference yield:

: 1365757-09-0
(S)-benzyl 2-((4S,5R)-2,2-dimethyl-5-tetradecyl-1,3-dioxolan-4-yl)aziridine-1-carboxylate

: 1365757-11-4
C₃₂H₄₉NO₄S

Guidance literature:: Multi-step reaction with 2 steps

1: 1,8-diazabicyclo[5.4.0]undec-7-ene / acetonitrile / 0.08 h / 100 °C / 5171.77 Torr / Inert atmosphere; CEM Discover Focused_.(TM). Microwave reactor; Sealed vessel

2: camphor-10-sulfonic acid / methanol / 20 °C

With camphor-10-sulfonic acid; 1,8-diazabicyclo[5.4.0]undec-7-ene; In methanol; acetonitrile;
DOI:10.1016/j.tetlet.2012.02.066