1-[3-(4-bromophenyl)-4,6-dimethoxy-2-methylindol-7-yl]-2,2,2-trifluoroethanone oxime

Base Information

Chemical Name:1-[3-(4-bromophenyl)-4,6-dimethoxy-2-methylindol-7-yl]-2,2,2-trifluoroethanone oxime
CAS No.:902772-57-0
Molecular Formula:C₁₉H₁₆BrF₃N₂O₃
Molecular Weight:457.247
Hs Code.:

Synonyms:1-[3-(4-bromophenyl)-4,6-dimethoxy-2-methylindol-7-yl]-2,2,2-trifluoroethanone oxime

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-[3-(4-bromophenyl)-4,6-dimethoxy-2-methylindol-7-yl]-2,2,2-trifluoroethanone oxime

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Technology Process of 1-[3-(4-bromophenyl)-4,6-dimethoxy-2-methylindol-7-yl]-2,2,2-trifluoroethanone oxime

There total 1 articles about 1-[3-(4-bromophenyl)-4,6-dimethoxy-2-methylindol-7-yl]-2,2,2-trifluoroethanone oxime which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 869960-00-9
3-(4-bromophenyl)-4,6-dimethoxy-2-methyl-7-trifluoroacetylindole

: 902772-57-0
1-[3-(4-bromophenyl)-4,6-dimethoxy-2-methylindol-7-yl]-2,2,2-trifluoroethanone oxime

Guidance literature:: With pyridine; hydroxylamine hydrochloride; In ethanol; for 24h; Heating;
DOI:10.1016/j.tet.2006.04.041

Reference yield: 100.0%

: 902772-57-0
1-[3-(4-bromophenyl)-4,6-dimethoxy-2-methylindol-7-yl]-2,2,2-trifluoroethanone oxime

: 70-34-8,65727-75-5
2,4-Dinitrofluorobenzene

: 902772-63-8
1-[-3-(4-bromophenyl)-4,6-dimethoxy-2-methylindol-7-yl]-2,2,2-trifluoroethanone O-(2,4-dinitrophenyl)oxime

Guidance literature:: With sodium ethanolate; In ethanol; at 20 ℃; for 0.5h;
DOI:10.1016/j.tet.2006.04.041

Reference yield:

: 902772-57-0
1-[3-(4-bromophenyl)-4,6-dimethoxy-2-methylindol-7-yl]-2,2,2-trifluoroethanone oxime

: 5-(4-bromophenyl)-6,8-dimethoxy-4-methyl-1-trifluoromethylpyrrolo[3,2,1-hi]indazole

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / NaOEt / ethanol / 0.5 h / 20 °C

2: 29 percent / sodium hydride / dioxane / 1 h / Heating

With sodium ethanolate; sodium hydride; In 1,4-dioxane; ethanol;
DOI:10.1016/j.tet.2006.04.041